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GB/T 29612-2013Carbon black - Determination of cadmium, lead, mercury content (English PDF)

炭黑中镉、铅、汞含量的测定

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Issued by

SAMR; SAC

Level / Type

National · Recommended

Issue date

July 19, 2013

Implementation date

December 1, 2013

Scope

GB/T 29612-2013 is the English-translated version of 炭黑中镉、铅、汞含量的测定.

GB/T 29612-2013 is the Chinese standard "Carbon black - Determination of cadmium, lead, mercury content".

Its scope clause reads: This standard specifies the method using an atomic absorption spectrophotometer (A method), plasma emission spectrometry method (B method) (Arbitration Law), X fluorescence spectrometry Meter method (C method), carbon black, cadmium (Cd), lead (Pb), Test Method for mercury (Hg) Determination.

This standard applies to carbon black. Its clauses include sampling; instrument; atomic absorption spectrophotometer (a method).

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Document preview — GB/T 29612-2013

National Standard of the People's Republic of China

ICS
83.040.20
Classification
G 49

Issued by: State Administration for Market Regulation; Standardization Administration of the PRC

Contents

  • 1 Scope
  • 2 Normative references
  • 3 Sampling
  • 4 Instrument
  • 5 atomic absorption spectrophotometer (A method)

1 Scope

This standard specifies the method using an atomic absorption spectrophotometer (A method), plasma emission spectrometry method (B method) (Arbitration Law), X fluorescence spectrometry

Meter method (C method), carbon black, cadmium (Cd), lead (Pb), Test Method for mercury (Hg) Determination.

This standard applies to carbon black.

2 Normative references

The following documents for the application of this document is essential. For dated references, only the dated version suitable for use herein

Member. For undated references, the latest edition (including any amendments) applies to this document.

GB 3778 carbon black for rubber

GB/T 3780.8 black - Part 8. Determination of loss on heating

Part 10 GB/T 3780.10 Carbon black. Determination of ash

Laboratory use specifications and test methods GB/T 6682 Analysis

GB 6819 acetylene

GB/T 12808 Laboratory glassware single marking pipette

3 Sampling

Carbon black according to the provisions of GB 3778 sampled.

4 Instrument

Conventional laboratory equipment and less equipment.

4.1

platinum crucible volume of about 35cm3.

4.2

Atomic absorption spectrophotometer equipped with an air/acetylene gas burner and cadmium, lead, mercury hollow cathode lamp.

4.3

plasma emission spectrometer.

4.4

X-ray fluorescence spectrometer.

4.5

Analytical balance with an accuracy of 0.1mg.

4.6

beaker with a volume of 100cm3.

4.7

flask, volume 100cm3,500cm3,1000cm3.

4.8

Single-marking pipette, capacity 1cm3,5cm3,10cm3,20cm3, should be consistent with GB/T 12808 in Class A requirements.

5 atomic absorption spectrophotometer (A method)

5.1 Test Method

After sample ashing, the residue was dissolved with hydrochloric acid, diluted inhaled flame atomic absorption spectrophotometer, respectively […]

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This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 15 pages — is available in the English PDF.

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