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GB/T 2679.11-2008Paper and board - qualitative analysis of mineral filler and mineral coating - SEM/EDAX method (English PDF)

纸和纸板中无机填料和无机涂料的定性分析 电子显微镜/X射线能谱法

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Issued by

SAMR; SAC

Level / Type

National · Recommended

Issue date

August 19, 2008

Implementation date

May 1, 2009

Scope

GB/T 2679.11-2008 is the English-translated version of 纸和纸板中无机填料和无机涂料的定性分析 电子显微镜/X射线能谱法.

GB/T 2679.11-2008 is the Chinese standard "Paper and board - qualitative analysis of mineral filler and mineral coating - SEM/EDAX method". Its scope clause reads: This section GB/T 2679 provisions of the electron microscopy/X-ray spectroscopy qualitative analysis of paper and paperboard coated with inorganic filler and inorganic Material way.

This section applies to an inorganic filler in paper and board coating composition of species identification and analysis, but also for papermaking inorganic filler, paint Analysis of raw materials. Its clauses include reagents and materials.

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Document preview — GB/T 2679.11-2008

National Standard of the People's Republic of China

ICS
85.010
Classification
Y 30
Replacing
GB/T 2679.11-1993

Issued by: State Administration for Market Regulation; Standardization Administration of the PRC

Contents

  • 1 Scope
  • 2 Normative references
  • 4 Reagents and materials
  • 4.2 hexametaphosphate [(NaPO3) 6]
  • 4.4 acetone (CH3COCH3)
  • 4.5 Concentrated hydrochloric acid (HCl)
  • 4.9 high-purity gold
  • 4.10 high purity carbon rod
  • 4.11 dichloroethylene (ClCH-CHCl)
  • 4.12 PVF (polyvinylformvar) of chloride solution

1 Scope

This section GB/T 2679 provisions of the electron microscopy/X-ray spectroscopy qualitative analysis of paper and paperboard coated with inorganic filler and inorganic

Material way.

This section applies to an inorganic filler in paper and board coating composition of species identification and analysis, but also for papermaking inorganic filler, paint

Analysis of raw materials.

2 Normative references

The following documents contain provisions which, through reference to GB/T 2679 to the present, constitute provisions of this section. For dated reference documents

Member, all subsequent amendments (not including errata content) or revisions do not apply to this section, however, encouraged to reach under this section

Parties to research agreement to use the latest versions of these documents. For undated reference documents, the latest versions apply to this section.

GB/T 450 and take samples to an aspect of paper and paperboard samples, positive and negative determination (GB/T 450-2008, ISO 186.

2002, MOD)

GB/T 742 paper-making raw material, pulp, paper and board Determination of ash (GB/T 742-2008, ISO 2144.1997, MOD)

Principle 3 3.1 papermaking fillers and coatings are typically inorganic talc, calcium carbonate, kaolin, titanium dioxide and barium sulfate. Using an electron microscope

Observe the particle morphology and crystal morphology, the fillers and coatings can be identified.

3.2

When the electron beam on the sample, it will stimulate the release of a characteristic X-ray, and the energy with different elements. The use of a lithium drift

Shift silicon detectors, this signal will be able to collect, sort through the computer, to achieve the purpose of analysis elements.

4 Reagents and materials

4.1

distilled or deionized water.

4.2 hexametaphosphate [(NaPO3) 6]

0.1% solution.

4.4 acetone (CH3COCH3)

chemically pure (clean electron microscopy and copper network).

4.5 Concentrated hydrochloric acid (HCl)

chemically pure (clean electron microscope dedicated copper network).

4.6

D76 developer.

4.7

D72 developer.

4.8

acidic fixer.

4.9 high-purity gold

purity of 99.99%, u00d81mm.

4.10 high purity carbon rod

the purity of 99.99%, u00d85mm × 100mm.

4.11 dichloroethylene (ClCH-CHCl)

chemically pure.

4.12 PVF (polyvinylformvar) of chloride solution

0.2% to 0.5% (mass fraction).

GB/T 2678.2-2021 | GB/T 2679.1-2020 | GB/T 1541-2013 | GB/T 2679.6-2026 | GB/T 2679.17-2026 | GB/T 2679.14-2026 | […]

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This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 15 pages — is available in the English PDF.

Similar standards

Editions of GB/T 2679.11

EditionTitleRevisionStatus
GB/T 2679.11-2008Paper and board - qualitative analysis of mineral filler and mineral coating - SEM/EDAX methodcurrent editionCurrent
GB/T 2679.11-1993Paper and board - qualitative analysis of mineral filler and mineral coating - SEM/EDAX methodprevious editionSuperseded

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