GB/T 24200-2009Determination of phenol and homologues contents of crude phenol (English PDF)
粗酚中酚及同系物含量的测定方法
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Issued by
SAMR; SAC
Level / Type
National · Recommended
Issue date
July 8, 2009
Implementation date
April 1, 2010
Scope
GB/T 24200-2009 is the English-translated version of 粗酚中酚及同系物含量的测定方法.
GB/T 24200-2009 is the Chinese standard "Determination of phenol and homologues contents of crude phenol". Its scope clause reads: This standard specifies the principles of the crude phenol and phenol homologues content determination, reagents and instruments, test procedures, the results of the calculation precision.
This standard applies to the determination of high temperature coal tar fractionation resulting crude phenol and its homologues of phenol content. Its clauses include test principle; reagents and instruments.
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Document preview — GB/T 24200-2009
National Standard of the People's Republic of China
- ICS
- 71.080.90
- Classification
- G 17
Issued by: State Administration for Market Regulation; Standardization Administration of the PRC
Contents
- 1 Scope
- 2 Normative references
- 3 Test principle
- 4 Reagents and Instruments
1 Scope
This standard specifies the principles of the crude phenol and phenol homologues content determination, reagents and instruments, test procedures, the results of the calculation precision.
This standard applies to the determination of high temperature coal tar fractionation resulting crude phenol and its homologues of phenol content.
2 Normative references
The following documents contain provisions which, through reference in this standard and become the standard terms. For cited documents with dates, with its
After all of the amendments (not including errata content) or revisions do not apply to this standard, however, encourage each agreement in accordance with this standard
Are Prescriptions can use the latest versions of these documents. For undated reference documents, the latest versions apply to this standard.
GB/T 8170 repair value expressed about the rules and limit values and judgment
YB/T 2305 coking products Glass thermometers
3 Test principle
Take a certain amount of sample, kerosene - xylene mixture as a substrate solution, distilled, evaporated after all distillate with a base effect generated sodium phenol,
Lye ml increments multiplied by its average density, in terms of the mass fraction of phenol and homologs. The reaction is as follows.
C6H5OH + NaOH -> C6H5ONa + H2O
4 Reagents and Instruments
4.1 Kerosene - xylene
5 parts of xylene was mixed with 3 parts kerosene (kerosene must first washed 30% sulfuric acid, according to the proportion of 1.1, after separation
10% sodium hydroxide and, according to the proportion of 1.1, after separation by distillation cut 200 °C ~ 300 °C distillate).
4.2 Toluene
AR.
4.3 Sodium chloride
AR, 400 °C burning dehydration 1h.
4.4 Sodium hydroxide solution
10% (mass fraction) solution, saturated with sodium chloride, the use of filtration.
4.5 retort
copper volume 150mL, wall thickness of not more than 2mm, shown in Figure 1.
Note. Allow the use of benzene retorts.
Millimeters
Figure 1 retort
GB/T 22053-2020 | GB/T 26026-2010 | GB/T 24768-2009 | GB/T 47270-2026 | GB/T 27563-2026 | GB/T 10668-2026 | […]
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This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 15 pages — is available in the English PDF.
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