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GB/T 22786-2008Determination of essential parameters of potassium perchlorate for use in fireworks and firecrackers (English PDF)

烟花爆竹用高氯酸钾关键指标的测定

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Issued by

General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China; Standardization Administration of China

Level / Type

National · Recommended

Issue date

December 30, 2008

Implementation date

September 1, 2009

Scope

GB/T 22786-2008 is the English-translated version of 烟花爆竹用高氯酸钾关键指标的测定.

GB/T 22786-2008 is the Chinese national standard on determination of essential parameters of potassium perchlorate for use in fireworks and firecrackers, in the field of chemical technology. The /T suffix marks it as a recommended standard: it is not compulsory by itself, but it becomes binding as soon as a contract, a tender or a customer specification calls it up - which in practice is how most foreign buyers meet it. It was issued on 30 December 2008 by the General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China; Standardization Administration of China, and has been in force since 1 September 2009. Classification: ICS 71.100.30, CCS Y88. This page is published from the official record of the standard held by the Chinese standards administration: the identification, the dates, the classification and the issuing body are taken from there. The clause text, the tables and the numeric limits are in the document itself, which is delivered complete in English translation.

Document preview — GB/T 22786-2008

National Standard of the People's Republic of China

ICS
71.100.30
Classification
Y88

Issued by: General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China; Standardization Administration of China

Contents

  • 1 Scope
  • 2 Normative references
  • 3.2 Determination of water-insoluble content
  • 3.2.3 Analysis of step

Foreword

Appendix A of this standard is an informative annex. The standard proposed by China National Light Industry Council. This standard by the National Standardization Technical Committee of fireworks. This standard was drafted. Guangxi CIQ fireworks testing center. The main drafters of this standard. Suppliers Jie, Wu Junyi, Yanjia Kun, Xiao rejuvenation. Fireworks with potassium perchlorate key indicators measuring

1 Scope

GB/T 22786-2008 is the Chinese national standard on determination of essential parameters of potassium perchlorate for use in fireworks and firecrackers, in the field of chemical technology. The /T suffix marks it as a recommended standard: it is not compulsory by itself, but it becomes binding as soon as a contract, a tender or a customer specification calls it up - which in practice is how most foreign buyers meet it. It was issued on 30 December 2008 by the General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China; Standardization Administration of China, and has been in force since 1 September 2009. Classification: ICS 71.100.30, CCS Y88. This page is published from the official record of the standard held by the Chinese standards administration: the identification, the dates, the classification and the issuing body are taken from there. The clause text, the tables and the numeric limits are in the document itself, which is delivered complete in English translation.

This standard specifies the fireworks with water-insoluble content of potassium perchlorate, pH, moisture absorption, moisture content, fineness, purity, chloride Determination of content, content and sodium chlorate content and qualitative identification of hypochlorite. This standard applies to fireworks with water-insoluble content of potassium perchlorate, pH, moisture absorption, moisture content, fineness, purity, chloride Qualitative identification of content, content and sodium chlorate Determination and hypochlorite.

2 Normative references

The following documents contain provisions which, through reference in this standard and become the standard terms. For dated references, subsequent Amendments (not including errata content) or revisions do not apply to this standard, however, encourage the parties to the agreement are based on research Whether the latest versions of these documents. For undated reference documents, the latest versions apply to this standard. Preparation of

GB/T 601 chemical reagent standard titration solution

GB/T 6003.1 woven wire mesh test sieve ( GB/T 6003.1-1997, neq ISO 3310-1.1990)

GB/T 6682 analytical laboratory use specifications and test methods ( GB/T 6682-2008, ISO 3696. 1987, MOD)

GB/T 8170 repair value expressed about the rules and limit values \u200b\u200band judgment

3.2 Determination of water-insoluble content

3.2.1 Principle After the sample was dissolved in water, filtered, and dried insolubles were weighed.

3.2.2 Instruments Conventional laboratory equipment and instruments and the following devices.

3.2.2.1 Drying oven. Controlled temperature 105 °C ± 2 °C.

3.2.2.2 Analytical balance. accuracy of 0.1mg. 3.2.2.3 4 emery core Crucible. volume 30mL. After pumping water sufficiently washed, dried at 105 °C 3h, after cooling spare.

3.2.2.4 filtration device set.

3.2.3 Analysis of step

3.2.3.1 Weigh about 10g sample, accurate to 0.1mg, dissolved in 300mL water, heated until dissolved.

3.2.3.2 sand core which has been weighed crucible mounted on the filtration device, the resulting test solution was poured into the sand core

3.2.3.1 crucible suction filtration. Beaker Material was attached to the wall under the water, then wash with warm water.

3.2.3.3 The sand core crucible at 105 °C dried 3h, removed and placed in a desiccator, cooled to room temperature and weigh. Two parallel determination Sample, the mean value.

3.2.4 Calculation Results The mass fraction of water insoluble to count 1, expressed in%, according to equation (1).

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This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 20 pages — is available in the English PDF.

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GB/T 22786-2008Determination of essential parameters of potassium perchlorate for use in fireworks and firecrackerscurrent editionCurrent

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