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GB/T 20760-2006Method for the determination of alpha-trenbolone, beta-trenbolone residues in bovine muscle, liver and kidney - LC-UV method and LC-MS-MS method (English PDF)

牛肌肉、肝、肾中的α-群勃龙、β-群勃龙残留量的测定 液相色谱-紫外检测法和液相色谱-串联质谱法

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Issued by

SAMR; SAC

Level / Type

National · Recommended

Issue date

December 31, 2006

Implementation date

March 1, 2007

Scope

GB/T 20760-2006 is the English-translated version of 牛肌肉、肝、肾中的α-群勃龙、β-群勃龙残留量的测定 液相色谱-紫外检测法和液相色谱-串联质谱法.

GB/T 20760-2006 is the Chinese standard "Method for the determination of alpha-trenbolone, beta-trenbolone residues in bovine muscle, liver and kidney - LC-UV method and LC-MS-MS method".

Its scope clause reads: This standard specifies the LC-UV method and LC-MS-MS method for the determination of alpha-trenbolone, beta-trenbolone residues in bovine muscle, liver and kidney.

This standard is applicable to the determination of alpha-trenbolone, beta-trenbolone residues in bovine muscle, liver and kidney. For the method detection limit of this standard: the detection limits of LC-UV method and LC-MS-MS method for the determination of alpha-trenbolone, beta-trenbolone are both 2µg/kg.

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Document preview — GB/T 20760-2006

National Standard of the People's Republic of China

Classification
X 04

Issued by: State Administration for Market Regulation; Standardization Administration of the PRC

Contents

  • Foreword i
  • 1 Scope
  • 2 Normative references
  • 3 Principle
  • 4 Reagents and materials
  • 5 Apparatus
  • 6 Preparation and preservation of specimen
  • 7 Determination procedures
  • 8 Result calculation
  • 9 Precision
  • Annex A (Informative) Liquid chromatogram of reference-materials
  • Annex B (Informative) Recovery rate

1 Scope

This standard specifies the LC-UV method and LC-MS-MS method for the determination of alpha-trenbolone, beta-trenbolone residues in bovine muscle, liver and kidney.

This standard is applicable to the determination of alpha-trenbolone, beta-trenbolone residues in bovine muscle, liver and kidney.

For the method detection limit of this standard: the detection limits of LC-UV method and LC-MS-MS method for the determination of alpha-trenbolone, beta-trenbolone are both 2µg/kg.

2 Normative references

The following normative documents contain provisions which, through reference in this text, constitute provisions of this standard. For dated references, subsequent amendments (excluding corrections), or revisions, of any of these publications do not apply to this standard. However parties to agreements based on this standard are encouraged to investigate the possibility of applying the most recent editions of the normative documents indicated below. For undated references, the latest edition of the normative document referred to applies.

GB/T 6379.1 Accuracy(trueness and precision)of measurement methods and results - Part 1: General principles and definitions (GB/T 6379.1-2004; ISO 5725-1: 1994, IDT)

GB/T 6379.2 Accuracy (trueness and precision) of measurement methods and results - Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method (GB/T 6379.2-2004; ISO 5725-2:1994, IDT)

GB/T 6682 Water for analytical laboratory use - Specification and test methods (GB/T 6682-1992; neq ISO 3696:1987) […]

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This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 15 pages — is available in the English PDF.

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