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GB/T 16484.18-2009Chemical analysis methods of rare earth chloride and light rare earth carbonate - Part 18: Determination of ignition loss content in light rare earth carbonate - Gravimetry (English PDF)

氯化稀土、碳酸轻稀土化学分析方法 第18部分:碳酸轻稀土中灼减量的测定 重量法

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Issued by

SAMR; SAC

Level / Type

National · Recommended

Issue date

October 30, 2009

Implementation date

May 1, 2010

Scope

GB/T 16484.18-2009 is the English-translated version of 氯化稀土、碳酸轻稀土化学分析方法 第18部分:碳酸轻稀土中灼减量的测定 重量法.

GB/T 16484.18-2009 is the Chinese standard "Chemical analysis methods of rare earth chloride and light rare earth carbonate - Part 18: Determination of ignition loss content in light rare earth carbonate - Gravimetry".

Its scope clause reads: GB/T 16484 This part specifies the determination of the light rare earth carbonate loss on ignition. This section applies to the determination of light rare earth carbonate ignition loss, the measurement range of 40.00% ~ 90.00%.

Principle 2 The sample was 950 °C burning, burning before using the sample and calculate the loss on ignition ignited mass difference. Its clauses include equipment; sample; calculation and presentation of analysis results.

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Document preview — GB/T 16484.18-2009

National Standard of the People's Republic of China

ICS
77.120.99
Classification
H 14
Replacing
GB/T 16484.18-1996

Issued by: State Administration for Market Regulation; Standardization Administration of the PRC

Contents

  • 1 Scope
  • 3 Equipment
  • 4 Sample
  • 6 Calculation and presentation of analysis results

1 Scope

GB/T 16484 This part specifies the determination of the light rare earth carbonate loss on ignition.

This section applies to the determination of light rare earth carbonate ignition loss, the measurement range of 40.00% ~ 90.00%.

Principle 2

The sample was 950 °C burning, burning before using the sample and calculate the loss on ignition ignited mass difference.

3 Equipment

3.1 Analysis of balance

a sense of the amount of 0.1mg.

3.2 high-temperature furnace

1000 °C.

3.3

a platinum crucible.

4 Sample

Weighing the sample immediately after the opening.

Step 5 Analysis

5.1 Sample

Table 1 sample was weighed, accurate to 0.0001g.

Table 1

Sample Sample volume/g

The dried sample relatively 3

Relatively moist sample 50 5.2 Determination of the number of

Weigh two samples were measured parallel to the mean value.

5.3 Determination

The sample (5.1) in a burned at 950 °C to constant weight in a platinum crucible, calcined at 950 °C 1h. The platinum crucible out, coolish, set

In the dryer to cool to room temperature. Call quality on an analytical balance, repeat the operation until the difference between two adjacent mass does not exceed 1mg.

6 Calculation and presentation of analysis results

According to equation (1) calculate the loss on ignition of the mass fraction (%).

W1 (loss on ignition) 1- m1 = m1 2 m1 × 100 (1)

Where.

M1 --- before burning a platinum crucible and sample mass, in grams (g);

......
This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 15 pages — is available in the English PDF.

Referenced standards

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Editions of GB/T 16484.18

EditionTitleRevisionStatus
GB/T 16484.18-2009Chemical analysis methods of rare earth chloride and light rare earth carbonate - Part 18: Determination of ignition loss content in light rare earth carbonate - Gravimetrycurrent editionCurrent
GB/T 16484.18-1996Chemical analysis methods of rare earth chloride and light rare earth carbonate - Part 18: Determination of ignition loss content in light rare earth carbonate - Gravimetryprevious editionSuperseded

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