GB/T 16484.18-2009Chemical analysis methods of rare earth chloride and light rare earth carbonate - Part 18: Determination of ignition loss content in light rare earth carbonate - Gravimetry (English PDF)
氯化稀土、碳酸轻稀土化学分析方法 第18部分:碳酸轻稀土中灼减量的测定 重量法
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Issued by
SAMR; SAC
Level / Type
National · Recommended
Issue date
October 30, 2009
Implementation date
May 1, 2010
Scope
GB/T 16484.18-2009 is the English-translated version of 氯化稀土、碳酸轻稀土化学分析方法 第18部分:碳酸轻稀土中灼减量的测定 重量法.
GB/T 16484.18-2009 is the Chinese standard "Chemical analysis methods of rare earth chloride and light rare earth carbonate - Part 18: Determination of ignition loss content in light rare earth carbonate - Gravimetry".
Its scope clause reads: GB/T 16484 This part specifies the determination of the light rare earth carbonate loss on ignition. This section applies to the determination of light rare earth carbonate ignition loss, the measurement range of 40.00% ~ 90.00%.
Principle 2 The sample was 950 °C burning, burning before using the sample and calculate the loss on ignition ignited mass difference. Its clauses include equipment; sample; calculation and presentation of analysis results.
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Document preview — GB/T 16484.18-2009
National Standard of the People's Republic of China
- ICS
- 77.120.99
- Classification
- H 14
- Replacing
- GB/T 16484.18-1996
Issued by: State Administration for Market Regulation; Standardization Administration of the PRC
Contents
- 1 Scope
- 3 Equipment
- 4 Sample
- 6 Calculation and presentation of analysis results
1 Scope
GB/T 16484 This part specifies the determination of the light rare earth carbonate loss on ignition.
This section applies to the determination of light rare earth carbonate ignition loss, the measurement range of 40.00% ~ 90.00%.
Principle 2
The sample was 950 °C burning, burning before using the sample and calculate the loss on ignition ignited mass difference.
3 Equipment
3.1 Analysis of balance
a sense of the amount of 0.1mg.
3.2 high-temperature furnace
1000 °C.
3.3
a platinum crucible.
4 Sample
Weighing the sample immediately after the opening.
Step 5 Analysis
5.1 Sample
Table 1 sample was weighed, accurate to 0.0001g.
Table 1
Sample Sample volume/g
The dried sample relatively 3
Relatively moist sample 50 5.2 Determination of the number of
Weigh two samples were measured parallel to the mean value.
5.3 Determination
The sample (5.1) in a burned at 950 °C to constant weight in a platinum crucible, calcined at 950 °C 1h. The platinum crucible out, coolish, set
In the dryer to cool to room temperature. Call quality on an analytical balance, repeat the operation until the difference between two adjacent mass does not exceed 1mg.
6 Calculation and presentation of analysis results
According to equation (1) calculate the loss on ignition of the mass fraction (%).
W1 (loss on ignition) 1- m1 = m1 2 m1 × 100 (1)
Where.
M1 --- before burning a platinum crucible and sample mass, in grams (g);
......
This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 15 pages — is available in the English PDF.
Referenced standards
Similar standards
Editions of GB/T 16484.18
| Edition | Title | Revision | Status |
|---|---|---|---|
| GB/T 16484.18-2009 | Chemical analysis methods of rare earth chloride and light rare earth carbonate - Part 18: Determination of ignition loss content in light rare earth carbonate - Gravimetry | current edition | Current |
| GB/T 16484.18-1996 | Chemical analysis methods of rare earth chloride and light rare earth carbonate - Part 18: Determination of ignition loss content in light rare earth carbonate - Gravimetry | previous edition | Superseded |
This page sells the current edition, GB/T 16484.18-2009. Earlier editions are listed for reference only.
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Related Standards
GB/T 16484.1-2009 — Chemical analysis methods for rare earth chloride and light rare earth carbonate - Part 1: Determination of the cerium oxide content - Ammonium ferrous sulfate titrimetry
GB/T 16484.10-2009 — Chemical analysis methods of rare earth chloride and light rare earth carbonate - Part 10: Determination of manganese oxide content - Flame atomic absorption spectrometry
GB/T 16484.11-2009 — Chemical analysis methods of rare earth chloride and light rare earth carbonate - Part 11: Determination of lead oxide content - Flame atomic absorption spectrometry
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