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GB/T 14634.6-2010Test methods of rare earth three-band phosphors for fluorescent lamps - Part 6: Determination of specific surface area (English PDF)

灯用稀土三基色荧光粉试验方法 第6部分:比表面积的测定

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Issued by

SAMR; SAC

Level / Type

National · Recommended

Issue date

August 9, 2010

Implementation date

May 1, 2011

Scope

GB/T 14634.6-2010 is the English-translated version of 灯用稀土三基色荧光粉试验方法 第6部分:比表面积的测定.

GB/T 14634.6-2010 is the Chinese national method for measuring the specific surface area of rare earth three-band phosphors for fluorescent lamps, and is Part 6 of the seven-part GB/T 14634 series.

It works by air permeability: at a set temperature a laminar air flow crosses a powder bed of fixed thickness, the volume of air is the integral of the flow rate over time, and the time the air takes to cross the bed gives the specific surface area.

The standard describes the surface area analyser and the balance reading to 0.001 g, how the instrument constant K is found from a weighed standard phosphor sample, and how the sample chamber is packed with perforated copper discs and filter paper.

It replaces GB/T 14634.6-2002, was issued on 9 August 2010 and has applied since 1 May 2011.

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Document preview — GB/T 14634.6-2010

National Standard of the People's Republic of China

ICS
77.120.99
Classification
H 14
Replacing
GB/T 14634.6-2002

Issued by: State Administration for Market Regulation; Standardization Administration of the PRC

Contents

  • Foreword
  • 1 Scope
  • 2 Principle of the method
  • 3 Instruments and apparatus

Foreword

GB/T 14634 "light rare earth trichromatic phosphors Test Method" is divided into seven sections.

--- Part 1. Determination of relative brightness;

--- Part 2. Determination of emission peak and color performance;

--- Part 3. Determination of thermal stability;

--- Part 4. Electric sensing particle size distribution measurement;

--- Part 5. Determination of density;

--- Part 6. Determination of specific surface area;

--- Part 7. Determination of thermal quenching.

Part is divided into 6 sections.

The partial revision of GB/T 14634.6-2002 "light rare earth trichromatic phosphors Test Method for Determination of specific surface area," the.

This section compared with the GB/T 14634.6-2002, the main changes are as follows.

--- Adjust some analysis condition;

--- Increasing the precision of the terms, adjusted the allowable difference;

--- Standard text made editorial changes.

Appendix A of this section is an informative annex.

This part of the National Standardization Technical Committee rare and centralized.

1 Scope

GB/T 14634 provisions of this part of the measurement method using light rare earth trichromatic phosphor surface area.

This section applies to light rare earth trichromatic phosphor surface area measurement.

2 Principle of the method

At a certain temperature, the laminar flow of air through the time required for a certain thickness of the powder bed and the surface area ratio of the powder into a certain functional relationships system. The amount of air flowing into a certain thickness of the powder bed is changing the flow rate for the time integral of the results. The air through the powder bed Time to the specific surface area of powder.

3 Instruments and apparatus

3.1 surface area analyzer (see Figure 1).

3.2 Balance. Precision 0.001g.

3.3 Determination of instrument constant K

3.3.1 Weigh phosphors standard sample (m0), accurate to 0.01g. Weigh the amount of porosity so that a standard sample (e0) in an appropriate range tightness Between, see equation (1).

3.3.2 In the bottom of the sample chamber into the first multi-well round copper, filter paper and then placed in a multi-hole circle with a diameter of copper, and copper in close agreement.

......
This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 15 pages — is available in the English PDF.

Similar standards

Editions of GB/T 14634.6

EditionTitleRevisionStatus
GB/T 14634.6-2010Test methods of rare earth three-band phosphors for fluorescent lamps - Part 6: Determination of specific surface areacurrent editionCurrent
GB/T 14634.6-2002Test methods of rare earth three-band phosphors for fluorescent lamps - Part 6: Determination of specific surface areaprevious editionSuperseded

This page sells the current edition, GB/T 14634.6-2010. Earlier editions are listed for reference only.

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