YS/T 798-2012Lithium nickel cobalt manganese oxide (English PDF)
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Issued by
Ministry of Industry and Information Technology of the PRC
Level / Type
National · Recommended
Issue date
May 24, 2012
Implementation date
November 1, 2012
Scope
YS/T 798-2012 (Lithium nickel cobalt manganese oxide) is available as an English-translated PDF.
YS/T 798-2012 — This Standard specifies the terms and definitions, requirements, test methods, inspection rules, marking, packaging, transportation, storage, quality certificate and contract (or order form) content of lithium nickel cobalt manganese oxide.
This Standard applies to lithium nickel cobalt manganese oxide as the positive active material for lithium ion batteries.
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Document preview — YS/T 798-2012
National Standard of the People's Republic of China
- ICS
- 77.160
- Classification
- H 71
Issued by: Ministry of Industry and Information Technology of the PRC
Contents
- Foreword...3
- 1 Scope...4
- 2 Normative references...4
- 3 Terms and definitions...5
- 4 Requirements...5
- 5 Test methods...7
- 6 Inspection rules...8
- 7 Marking, packaging, transportation, storage and quality certificate...10
- 8 Contract (or order form) content...11
Foreword
This Standard is drafted in accordance with the rules given in GB/T 1.1-2009.
This Standard shall be under the jurisdiction of National Technical Committee
243 on Nonferrous Metals of Standardization Administration of China (SAC/TC
243).
Responsible drafting organization of this Standard. Wujie Science &
Technology Co., Ltd.
Participating drafting organizations of this Standard. Shenzhen Tianjiao
Technology Development Co., Ltd., Guangdong Brunp Recycling Technology
Co., Ltd., CITIC Guoan Mengguli Power Technology Co., Ltd., Beijing Easpring
Material Technology Co., Ltd.
Main drafters of this Standard. Jiang Ning, Jiang Yongshan, He Zhaoshu, Li
Junfeng, Wang Weidong, Li Changdong, Zhu Xiaopei, Chen Yanbin.
Lithium nickel cobalt manganese oxide
1 Scope
This Standard specifies the terms and definitions, requirements, test methods,
inspection rules, marking, packaging, transportation, storage, quality certificate
and contract (or order form) content of lithium nickel cobalt manganese oxide.
This Standard applies to lithium nickel cobalt manganese oxide as the positive
active material for lithium ion batteries.
2 Normative references
The following documents are indispensable for the application of this document.
For the dated references, only the editions with the dates indicated are
applicable to this document. For the undated references, the latest edition
(including all the amendments) are applicable to this document.
GB/T 1717 Determination of pH value of an aqueous suspension of pigments
GB/T 5162 Metallic powders - Determination of tap density
GB/T 5314 Powders for powder metallurgical purposes - Sampling
GB/T 6283 Chemical products - Determination of water Karl - Fischer method
(general method)
GB/T 19077.1 Particle size analysis - Laser diffraction methods - Part 1.
General principles
GB/T 19587 Determination of the specific surface area of solids by gas
adsorption using the BET method
GB/T 20252-2006 Lithium cobalt oxide
GB/T 23365 Electrochemical performance test of lithium cobalt oxide - Test
method for specific capacity and charge-discharge efficiency of the first cycle
3 Terms and definitions
The terms and definitions in GB/T 20252-2006 apply to this document.
4 Requirements
4.1 Chemical composition
4.2 Appearance quality
The appearance of the product shall be gray-black powder, with uniform color,
no agglomeration, and no inclusions.
4.3 Crystal structure
The crystal structure of the product shall comply with the JCPDS standard (09-0063).
4.4 Physical properties
4.4.1 Tap density
The tap density of the product is not less than 1.8 g/cm3.
4.5 pH value
The pH value of the product is not more than 10.0~12.5.
4.6 Electrochemical performance
4.6.1 First discharge specific capacity
The first discharge specific capacity of the product under the specified
conditions shall not be less than 140 mA · h/g.
4.6.2 First charge-discharge efficiency
4.7 Other requirements
If the purchaser has special requirements for lithium nickel cobalt manganese
oxide, it can be negotiated between the supplier and the purchaser.
5 Test methods
5.1 Chemical composition
5.2 Appearance quality
The appearance quality of the product is inspected visually.
5.3 Crystal structure
The crystal structure of the product is detected using an X-ray powder
diffractometer.
5.4 Physical properties
5.4.1 Tap density
The tap density of the product is determined in accordance with the provisions
of GB/T 5162.
5.5 pH value
The pH value of the product is determined in accordance with the provisions of
GB/T 1717.
5.6 Electrochemical performance
5.6.1 First discharge specific capacity
The first discharge specific capacity of the product is determined with reference
to the regulations of GB/T 23365.
5.6.2 First charge-discharge efficiency
6 Inspection rules
6.1 Inspection and acceptance
6.1.1 The product shall be inspected by the supplier. It shall be ensured that the
product quality meets the requirements of this Standard and the contract (or
order form). It shall fill in the product quality certificate.
6.2 Lot grouping
Products shall, in lots, be submitted for acceptance. Each lot shall be composed
of the same mixture. The weight of each lot shall not be greater than 5 t.
6.3 Inspection items and sampling
6.4 Determination of inspection results
6.4.1 If one of the product's chemical composition, water, molar ratio of Li to
Ni+Co+Mn content in the chemical composition, crystal structure, tap density,
particle size distribution, specific surface area, and pH value is nonconformity,
the lot is judged to be nonconformity.
6.4.2 If the inspection of appearance quality is nonconformity, this drum of
products is judged to be nonconformity.
6.4.3 According to the method specified in GB/T 23365, make 6 test batteries.
3 of them are randomly selected for the inspection of first discharge specific
capacity and first charge-discharge efficiency. If the performance of 2 batteries
fails to meet the requirements of this Standard, it is allowed to take another 3
batteries for repeated tests. If there are still 2 batteries whose performance does
not meet the requirements of this Standard, the lot is deemed nonconformity.
7 Marking, packaging, transportation, storage and quality certificate
7.1 Marking
A label card shall be affixed on the outer packaging, which shall indicate.
7.2 Packaging
For products that have passed the inspection, 25 kg is a packaging unit. The
inner packaging is a composite aluminum-plastic bag.
7.3 Transportation and storage
Products, packaged in accordance with 7.2, can be transported in various ways.
But it shall avoid damaging the packaging and making the product damp. The
product shall be stored in a dry and non-corrosive environment. From the date
of production, the product has a shelf life of 2 years.
7.4 Quality certificate
Each lot of products shall be accompanied by a quality certificate, which shall
indicate.
8 Contract (or order form) content
The contract (or order form) for ordering the products listed in this Standard
shall include the following.
YS/T 798-2012
YS
NONFERROUS METAL INDUSTRY STANDARD
ICS 77.160
H 71
Lithium nickel cobalt manganese oxide
Issued on. MAY 24, 2012
Implemented on. NOVEMBER 01, 2012
Issued by. Ministry of Industry and Information Technology of the PRC
Table of Contents
Foreword... 3
1 Scope... 4
2 Normative references... 4
3 Terms and definitions... 5
4 Requirements... 5
5 Test methods... 7
6 Inspection rules... 8
7 Marking, packaging, transportation, storage and quality certificate... 10
8 Contract (or order form) content... 11
Foreword
This Standard is drafted in accordance with the rules given in GB/T 1.1-2009.
This Standard shall be under the jurisdiction of National Technical Committee
243 on Nonferrous Metals of Standardization Administration of China (SAC/TC
243).
Responsible drafting organization of this Standard. Wujie Science &
Technology Co., Ltd.
Participating drafting organizations of this Standard. Shenzhen Tianjiao
Technology Development Co., Ltd., Guangdong Brunp Recycling Technology
Co., Ltd., CITIC Guoan Mengguli Power Technology Co., Ltd., Beijing Easpring
Material Technology Co., Ltd.
Main drafters of this Standard. Jiang Ning, Jiang Yongshan, He Zhaoshu, Li
Junfeng, Wang Weidong, Li Changdong, Zhu Xiaopei, Chen Yanbin.
Lithium nickel cobalt manganese oxide
1 Scope
This Standard specifies the terms and definitions, requirements, test methods,
inspection rules, marking, packaging, transportation, storage, quality certificate
and contract (or order form) content of lithium nickel cobalt manganese oxide.
This Standard applies to lithium nickel cobalt manganese oxide as the positive
active material for lithium ion batteries.
2 Normative references
The following documents are indispensable for the application of this document.
For the dated references, only the editions with the dates indicated are
applicable to this document. For the undated references, the latest edition
(including all the amendments) are applicable to this document.
GB/T 1717 Determination of pH value of an aqueous suspension of pigments
GB/T 5162 Metallic powders - Determination of tap density
GB/T 5314 Powders for powder metallurgical purposes - Sampling
GB/T 6283 Chemical products - Determination of water Karl - Fischer method
(general method)
GB/T 19077.1 Particle size analysis - Laser diffraction methods - Part 1.
General principles
GB/T 19587 Determination of the specific surface area of solids by gas
adsorption using the BET method
GB/T 20252-2006 Lithium cobalt oxide
GB/T 23365 Electrochemical performance test of lithium cobalt oxide - Test
method for specific capacity and charge-discharge efficiency of the first cycle
3 Terms and definitions
The terms and definitions in GB/T 20252-2006 apply to this document.
4 Requirements
4.1 Chemical composition
4.2 Appearance quality
The appearance of the product shall be gray-black powder, with uniform color,
no agglomeration, and no inclusions.
4.3 Crystal structure
The crystal structure of the product shall comply with the JCPDS standard (09-0063).
4.4 Physical properties
4.4.1 Tap density
The tap density of the product is not less than 1.8 g/cm3.
4.5 pH value
The pH value of the product is not more than 10.0~12.5.
4.6 Electrochemical performance
4.6.1 First discharge specific capacity
The first discharge specific capacity of the product under the specified
conditions shall not be less than 140 mA · h/g.
4.6.2 First charge-discharge efficiency
4.7 Other requirements
If the purchaser has special requirements for lithium nickel cobalt manganese
oxide, it can be negotiated between the supplier and the purchaser.
5 Test methods
5.1 Chemical composition
5.2 Appearance quality
The appearance quality of the product is inspected visually.
5.3 Crystal structure
The crystal structure of the product is detected using an X-ray powder
diffractometer.
5.4 Physical properties
5.4.1 Tap density
The tap density of the product is determined in accordance with the provisions
of GB/T 5162.
5.5 pH value
The pH value of the product is determined in accordance with the provisions of
GB/T 1717.
5.6 Electrochemical performance
5.6.1 First discharge specific capacity
The first discharge specific capacity of the product is determined with reference
to the regulations of GB/T 23365.
5.6.2 First charge-discharge efficiency
6 Inspection rules
6.1 Inspection and acceptance
6.1.1 The product shall be inspected by the supplier. It shall be ensured that the
product quality meets the requirements of this Standard and the contract (or
order form). It shall fill in the product quality certificate.
6.2 Lot grouping
Products shall, in lots, be submitted for acceptance. Each lot shall be composed
of the same mixture. The weight of each lot shall not be greater than 5 t.
6.3 Inspection items and sampling
6.4 Determination of inspection results
6.4.1 If one of the product's chemical composition, water, molar ratio of Li to
Ni+Co+Mn content in the chemical composition, crystal structure, tap density,
particle size distribution, specific surface area, and pH value is nonconformity,
the lot is judged to be nonconformity.
6.4.2 If the inspection of appearance quality is nonconformity, this drum of
products is judged to be nonconformity.
6.4.3 According to the method specified in GB/T 23365, make 6 test batteries.
3 of them are randomly selected for the inspection of first discharge specific
capacity and first charge-discharge efficiency. If the performance of 2 batteries
fails to meet the requirements of this Standard, it is allowed to take another 3
batteries for repeated tests. If there are still 2 batteries whose performance does
not meet the requirements of this Standard, the lot is deemed nonconformity.
7 Marking, packaging, transportation, storage and quality certificate
7.1 Marking
A label card shall be affixed on the outer packaging, which shall indicate.
7.2 Packaging
For products that have passed the inspection, 25 kg is a packaging unit. The
inner packaging is a composite aluminum-plastic bag.
7.3 Transportation and storage
Products, packaged in accordance with 7.2, can be transported in various ways.
But it shall avoid damaging the packaging and making the product damp. The
product shall be stored in a dry and non-corrosive environment. From the date
of production, the product has a shelf life of 2 years.
7.4 Quality certificate
Each lot of products shall be accompanied by a quality certificate, which shall
indicate.
8 Contract (or order form) content
The contract (or order form) for ordering the products listed in this Standard
shall include the following.
......
......
This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 11 pages — is available in the English PDF.
Referenced standards
Normative references
- GB/T 5162Metallic powders - Determination of tap density
- GB/T 5314Powders for powder metallurgical purposes -- Sampling
- GB/T 6283Chemical products -- Determination of water Karl-Fischer method (general method)
- GB/T 19587Determination of the specific surface area of solids by gas adsorption using the BET method
- GB/T 20252-2006Lithium cobalt oxide
- GB/T 23365Electrochemical performance test of lithium cobalt oxide - Test method for the initial discharge specific capacity and the initial efficiency
GB/T 1717 · GB/T 19077.1
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