SN/T 3056.3-2011rmination of essential parameters of chemical raw materials for use in fireworks and firecracker. Part 3: Lead tetraoxide powder (English PDF)
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Issued by
General Administration of Customs
Level / Type
National · Recommended
Issue date
September 9, 2011
Implementation date
April 1, 2012
Scope
SN/T 3056.3-2011 (rmination of essential parameters of chemical raw materials for use in fireworks and firecracker. Part 3: Lead tetraoxide powder) is available as an English-translated PDF.
SN/T 3056.3-2011 — SN/T 3056 provisions of this part of the fireworks with the determination of lead content of red lead, lead oxide content determination, carbon Determination of lead content, determination of nitrate content of insoluble matters, measurement method of iron content, moisture content and particle size test methods.
This section applies to the determination of fireworks with a lead content of red lead, lead oxide content determination, of the content of lead dioxide, nitric acid is not Determination of soluble matter content, Determination of iron content determination, moisture content and particle size determination.
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Document preview — SN/T 3056.3-2011
National Standard of the People's Republic of China
- Classification
- Y 88
Issued by: General Administration of Customs
Contents
- Foreword
- 1 Scope
- 2 Normative references
- 3 Determination
- 3.1 Drying the sample
- 3.2 Determination of insoluble matter content nitrate
Foreword
"Determination of fireworks with chemical raw materials key indicators" SN/T 3056 series of standards is divided into 15 parts.
--- Part 1. potassium hydrogen phthalate;
--- Part 2. sodium fluoride;
--- Part 3. Red Lead;
--- Part 4. basic copper carbonate;
--- Part 5. sulfur;
--- Part 6. strontium sulfate;
--- Part 7. copper sulfate;
--- Part 8. potassium chlorate;
--- Part 9. sodium bicarbonate;
--- Part 10. strontium carbonate;
--- Part 11. iron;
--- Part 12. barium nitrate;
--- Part 13. Silver nitrate;
--- Part 14. bismuth oxide;
--- Part 15. potassium dichromate.
This section SN/T 3056 Part 3.
This section drafted in accordance with GB/T 1.1-2009 given rules.
This section proposed and managed by the National Certification and Accreditation Administration Committee.
1 Scope
SN/T 3056 provisions of this part of the fireworks with the determination of lead content of red lead, lead oxide content determination, carbon Determination of lead content, determination of nitrate content of insoluble matters, measurement method of iron content, moisture content and particle size test methods.
This section applies to the determination of fireworks with a lead content of red lead, lead oxide content determination, of the content of lead dioxide, nitric acid is not Determination of soluble matter content, Determination of iron content determination, moisture content and particle size determination.
2 Normative references
The following documents for the application of this document is essential. For dated references, only the dated version suitable for use herein Member. For undated references, the latest edition (including any amendments) applies to this document.
Preparation of GB/T 601 chemical reagent standard titration solution General Method GB/T 3049 Industrial chemicals determination of iron content 1,10 phenanthroline spectrophotometry Lynn GB/T 6003.1 woven wire mesh test sieve (GB/T 6003.1-1997, ISO 3310-1:1990, NEQ) GB/T 6003.2 Test sieves of perforated metal plate (GB/T 6003.2-1997, ISO 3310-2:1990, NEQ) GB/T 6003.3 electroformed sheet test sieve (GB/T 6003.3-1999, ISO 3310-3:1990, NEQ) GB/T 6005 Test sieves - Metal wire cloth, perforated plate, electrical sheet - basic mesh size (GB/T 6005-1997, ISO 565:1990, NEQ) Laboratory use specifications and test methods GB/T 6682 Analysis GB/T 8170 repair value expressed about the rules and limit values and judgment
3 Determination
3.1 Drying the sample
Sample at 105 °C ± 2 °C dried 3h, into the dryer to cool reserve. After drying the sample project to detect water points outside use.
3.2 Determination of insoluble matter content nitrate
3.2.1 Principle
Sample with nitric acid and hydrogen peroxide dissolved was filtered, dried insolubles, call quality.
3.2.2 Reagents
Unless otherwise indicated in the analysis using only confirm at least three water analytical grade reagents and GB/T 6682 stipulated.
3.2.2.1 nitric acid (12).
3.2.2.2 Hydrogen peroxide (30%).
......
This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 7 pages — is available in the English PDF.
Referenced standards
Normative references
- GB/T 601Chemical Reagent - Preparations of Standard Volumetric Solutions
- GB/T 3049Chemical products for industrial use - General method for determination of iron content. 1, 10-Phenanthroline spectrophotometric method
- GB/T 6003.1Test sieves—Technical requirements and testing—Part 1:Test sieves of metal wire cloth
- GB/T 6003.1-1997Test sieves—Technical requirements and testing—Part 1:Test sieves of metal wire cloth
- GB/T 6003.2Test sieves - Technical requirements and testing - Part 2: Test sieves of perforated metal plate
- GB/T 6003.2-1997Test sieves - Technical requirements and testing - Part 2: Test sieves of perforated metal plate
ISO 3310 · GB/T 6003.3 · GB/T 6003.3-1999 · ISO 565
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GB/T 3049-2006 — Chemical products for industrial use - General method for determination of iron content. 1, 10-Phenanthroline spectrophotometric method
GB/T 30491.1-2014 — Natural gas -- Calculation of thermodynamic properties -- Part l: Gas phase properties for transmission and distribution applications
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