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SN/T 0001-2016Rules for standards of physical and chemical analysis method for the determination in food and cosmetics for export (English PDF)

出口食品、化妆品理化测定方法标准编写的基本规定

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Issued by

General Administration of Customs

Level / Type

National · Recommended

Issue date

March 9, 2016

Implementation date

October 1, 2016

Scope

SN/T 0001-2016 is the English-translated version of 出口食品、化妆品理化测定方法标准编写的基本规定.

SN/T 0001-2016 — This standard stipulates the requirements for the preparation of physics and chemistry methods for foods and cosmetics and the preparation requirements for their formulation, presentation rules, and standard setting.

Technical specifications.

This standard applies to pesticide residues in food and cosmetics, veterinary drug residues, biological toxins, chemical elements, persistent environmental pollutants, food additives Preparation of standards for determination of physical and chemical indicators such as additives and nutrients; applicable to physical and chemical indicators such as prohibited substances and chemical elements in cosmetics the preparation of standard methods.

The standard for the physicochemical determination of feed and the requirements for the preparation of the preparation instructions, the expression rules, and the specifications of the standard formulation, may refer to this standard is implemented.

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Document preview — SN/T 0001-2016

National Standard of the People's Republic of China

Classification
X 04;Y42
Replacing
SN/T 0001-1995

Issued by: General Administration of Customs

Contents

  • Foreword
  • 1 Scope
  • 2 Normative references
  • 3 Terms and Definitions
  • 4 General requirements
  • 5 Writing standard
  • 5.1 Structure and Writing Sequence
  • 5.2 Informational Overview Element
  • 5.2.1 Cover
  • 5.2.2 Goal
  • 5.2.3 Preface
  • 5.2.4 Introduction
  • 5.3 Normative General Elements
  • 5.3.1 Standard Name
  • 5.3.2 Range
  • 5.3.3 Normative references
  • 5.4 Normative Technical Elements
  • 5.4.1 Terms and Definitions
  • 5.4.2 Method Summary
  • 5.4.3 Reagents and Materials
  • 5.4.3.1 General requirements
  • 5.4.3.2 Arrangement order
  • 5.4.3.2.1 General
  • 5.4.3.2.2 Products used in the market
  • 5.4.3.2.3 Formulation solution
  • 5.4.3.2.4 Standard titration solution
  • 5.4.3.2.5 Standard solution
  • 5.4.3.2.6 Indicator
  • 5.4.3.2.7 Auxiliary material
  • 5.4.4 Instruments and Equipment
  • 5.4.5 Measurement Step
  • 5.4.5.1 Extraction
  • 5.4.5.2 Purification
  • 5.4.5.3 Determination
  • 5.4.6 Result Calculation and Presentation
  • 5.4.7 Limit of quantification
  • 5.4.8 Accuracy (Recovery)
  • 5.4.9 Normative Appendix
  • 5.5 Informative supplementary elements
  • 5.5.1 Informative Appendix
  • 5.5.2 Reference
  • 5.5.3 Index
  • 5.6 Other rules
  • 5.6.1 Quantity, Units and Symbols
  • 5.6.2 Chemical Name
  • 5.6.3 Figure
  • 5.6.4 Table
  • 6 Preparation of preparation instructions
  • 6.1 Task Source
  • 6.2 Significance and Characteristics of Standard Setting
  • 6.3 Basis for standard preparation
  • 6.4 The main process of standard setting
  • 6.5 Method Technical Demonstration
  • 6.6 Map
  • 6.7 Collaborative Experiments
  • 6.8 Summary of Solicitation
  • 6.9 Attachment Requirements
  • 6.10 Other issues that need to be explained
  • 7 Standard Verification Requirements
  • 7.1 Validation Laboratory Qualification
  • 7.2 Validation Laboratory Selection
  • 7.3 Authentication Parameter Selection
  • 8 Technical requirements for standard setting
  • 8.1 Qualitative Requirements
  • 8.1.1 Specificity
  • 8.1.1.1 Specificity of Residue Analysis Method
  • 8.1.1.2 Specificity of Component Identification Methods
  • 8.1.1.3 Specificity of Content Determination and Impurity Determination Method
  • 8.1.2 Detection limit
  • 8.2 Quantitative Requirements
  • 8.2.1 Limit of quantification
  • 8.2.2 Accuracy
  • 8.3 Precision
  • 8.3.1 General Requirements
  • 8.3.2 Expression
  • 8.3.3 Repeatability Test
  • 8.3.4 Reproducibility Test
  • 8.4 Quantitative Methods
  • 8.4.1 Standard Curve Method
  • 8.4.2 Single Point Method
  • 8.5 Additional Technical Requirements for Validation Methods
  • 8.6 Robustness
  • 8.7 Target Analyte Stability
  • 8.7.1 General requirements
  • 8.7.2 Stability of analytes in solution
  • 8.7.3 Stability of Analytes in the Matrix
  • Appendix A (Informative) Food Category Regulations for Preparing Standards for Determination of Chemical Contaminants and Additives in Import and Export of Food
  • A.1 Classification Principle
  • A.2 Classification
  • A.2.1 Animal source food
  • A.2.2 Plant-derived foods
  • A.2.3 Processed Food
  • Appendix B (Normative) Additional Technical Requirements for Validation Methods
  • B.1 Additional Performance Standards and Other Requirements for Methods for Quantitative Analysis of Organic Residues and Contaminants
  • B.1.1 Performance Standards and Other Requirements for Chromatography-Mass Spectrometry Detection
  • B.1.2 Performance standards and other requirements for the determination of analytes by LC in conjunction with other detection techniques
  • B.2 Additional Performance Standards and Other Requirements for Chemical Element Quantification Methods
  • B.2.1 Atomic Absorption Spectroscopy (AAS) Requirements
  • B.2.2 Requirements for Flame Atomic Absorption Spectroscopy (AAS)
  • B.2.3 Requirements for Graphite Furnace Atomic Absorption Spectroscopy (AAS)
  • B.2.4 Specific requirements for hydride generation atomic absorption spectroscopy
  • B.2.5 Specific requirements for cold vapor atomic absorption spectroscopy
  • B.2.6 Specific requirements for inductively coupled plasma atomic emission spectrometry (ICP-AES)
  • B.2.7 Specific requirements for inductively coupled mass spectrometry (ICP-MS)
  • Reference

Foreword

This standard was drafted in accordance with the rules given in GB/T 1.1-2009.

This standard supersedes SN/T 0001-1995 "The standard for the preparation of standards for pesticides, veterinary drug residues and biotoxins in export commodities.

Compared with SN/T 0001-1995, the main technical changes of this provision, in addition to editorial changes, are as follows.

--- This revision basically retained the core part of SN/T 0001-1995;

--- In the standard structure, SN/T 0001-1995 "6.4 Sampling and preparation of samples" was deleted, adding "orders" "terms and definitions" and "reference" three optional elements;

--- The scope of application of the standard is expanded except for the determination of pesticides, veterinary drug residues and biological toxins specified in SN/T 0001-1995 in addition to the preparation of standards, it also applies to standards for chemical elements, persistent environmental pollutants, food additives, and nutrient composition determination methods.

Write (see Chapter 1);

--- Changed SN/T 0001-1995 "3 Basic Requirements" to "4 Overall Requirements" and added "4.2 The formulation of this standard should be Meet SN/T 4530 requirements" (see Chapter 4);

--- In accordance with the provisions of GB/T 1.1-2009, combined with the actual needs of the SN standard, a more detailed description of the preparation of the various elements Provisions and examples one by one (see 5.2~5.5);

--- Increased specifications for quantities, units and symbols, chemical substance names, figures and tables (see 5.6);

--- Increased requirements for preparation of preparation instructions (see Chapter 6);

---Increase the specification requirements for standardization, merge the contents of Appendix A of SN/T 0001-1995 into Chapter 8, and press the latest international requirements are regulated again (see Chapter 8);

---The goods in Appendix B of SN/T 0001-1995 were reclassified into "chemical contaminants and additives in imported and exported foods." Formulation of Food Category Regulations for Preparation of Additives (see Appendix A).

This standard is proposed and managed by the National Certification and Accreditation Regulatory Commission.

1 Scope

This standard stipulates the requirements for the preparation of physics and chemistry methods for foods and cosmetics and the preparation requirements for their formulation, presentation rules, and standard setting.

Technical specifications.

This standard applies to pesticide residues in food and cosmetics, veterinary drug residues, biological toxins, chemical elements, persistent environmental pollutants, food additives Preparation of standards for determination of physical and chemical indicators such as additives and nutrients; applicable to physical and chemical indicators such as prohibited substances and chemical elements in cosmetics the preparation of standard methods.

The standard for the physicochemical determination of feed and the requirements for the preparation of the preparation instructions, the expression rules, and the specifications of the standard formulation, may refer to this standard is implemented.

2 Normative references

The following documents are indispensable for the application of this document. For dated references, only dated versions apply to this article Pieces. For undated references, the latest version (including all amendments) applies to this document.

GB/T 1.1-2009 Guidelines for Standardization Work Part 1. Structure and Writing of Standards (ISO/IEC Directives-Part 2.

2004, NEQ)

GB 3100 International System of Units and Its Application (GB 3100-1993, eqvISO 1000.1992) GB/T 3101 General principles for quantities, units and symbols (GB/T 3101-1993, eqvISO 31-0.1992) GB/T 3102 (all parts) quantity and unit [eqvISO 31 (all parts)] GB/T 6379.1 Accuracy (trueness and precision) of measurement methods and results Part 1. General rules and definitions, (GB/T 6379.1-2004, ISO 5725-1:1994, IDT) GB/T 6682 Analytical laboratory water specification and test methods (GB/T 6682-2008, ISO 3696:1987, MOD) GB/T.20000.2 Standardization Work Guide Part 2. Adoption of International Standards (GB/T.20000.2-2009, ISO/IEC Guide 21-1..2005, MOD) GB/T.20001.1 standard writing rules Part 1. Terminology (GB/T.20001.1-2001, ISO 10241:1992, NEQ) GB/T.20001.4 standard writing rules Part 4. Chemical analysis methods General requirements for GB/T 27025 testing and calibration laboratory capabilities (GB/T 27025-2008, ISO/IEC 17025:2005, IDT) SN/T 4530 Import and Export Food and Cosmetic Inspection Professional Standard System

3 Terms and Definitions

The terms and definitions defined in GB/T 1.1-2009, GB/T.20001.1, GB/T.20001.4 and GB/T 6379.1 and the following apply in this document. For ease of use, the following repeatedly lists some terms and definitions in GB/T 6379.1.

Limit of detection limit of detection, LOD the minimum concentration at which an analyte can be detected, that is, within a certain degree of confidence, the qualitative determination of the smallest analyte in a sample by a certain method

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This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 28 pages — is available in the English PDF.

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