SN 0590-1996Determination of pyrazon residues in meat and meat products for export. GC method (English PDF)

Foreword

This standard was drafted in accordance with GB/T 1.1-2009 given rules.

This standard replaces SN 0590-1996 "export of meat and meat products for residues of 2,4-D butyl ester method." this standard compared with SN 0590-1996, major technical changes are as follows.

--- Standard name from the "export of meat and meat products for 2,4-D butyl ester residues in" to "export meat and meat products 2,4 Butylate Residues by Gas Chromatography and Gas Chromatography - Mass Spectrometry ";

--- Expand the scope of the standard testing;

--- Deletion of a portion of the sample;

--- Improved sample preparation techniques;

--- Increased by gas chromatography - mass spectrometry method was confirmed;

--- Reducing the lower limit of detection, and detection of different objects, given the recovery of different substrates by adding different concentrations of the standard substance range.

This standard is proposed and managed by the National Certification and Accreditation Administration Committee.

This standard was drafted. People's Republic of China Shandong CIQ.

1 Scope

This standard specifies the export of meat and meat products for 2,4-D butyl Residues of sample preparation, gas chromatography and gas chromatography - mass spectroscopy Fixed and confirmation methods.

This standard applies to exports of chicken, pork, beef and pork sausages in 2,4-butyl residues in the detection and confirmation.

This method of measuring the low limit of 0.005mg/kg.

2 Normative references

The following documents for the application of this document is essential. For dated references, only the dated version suitable for use herein Member. For undated references, the latest edition (including any amendments) applies to this document.

Laboratory use specifications and test methods GB/T 6682 Analysis

3 Sample Preparation and Storage

Take a representative portion of the sample of about 500g, mix well with mashed masher organizations are divided into two, respectively, into a clean container as a Sample, sealed and marked with tags. The sample was placed in -18 °C stored.

4 Determination