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GB/T 47093-2026Chemical analysis methods for alumina fibre (English PDF)

氧化铝纤维化学分析方法

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Issued by

SAMR; SAC

Level / Type

National · Recommended

Issue date

January 28, 2026

Implementation date

August 1, 2026

Scope

GB/T 47093-2026 is the English-translated version of 氧化铝纤维化学分析方法.

GB/T 47093-2026 is the Chinese national standard covering the composition of alumina fibre - the alumina and silica proportions that decide its crystalline phase and its use temperature, and the alkali and iron impurities that lower both. It is the fibre of high-temperature furnace linings and of ceramic matrix composites. First edition, 19,000 words, published with GB/T 47086-2026 on fibre diameter. It was issued on 28 January 2026 and has been in force since 1 August 2026, as a first edition. The document is under the responsibility of the China Building Materials Federation. This page is published from the official record of the 2026 edition; the clause text of a standard this recent is not yet in circulation, and the figures, limits and tables it contains are those of the document itself, delivered in full with the English translation.

Document preview — GB/T 47093-2026

National Standard of the People's Republic of China

ICS
59.100.10
Classification
Q 36

Issued by: State Administration for Market Regulation; Standardization Administration of the PRC

Contents

  • 1.Scope1
  • 2 Normative References1
  • 3.Terms and Definitions1
  • 4 General Rules1
  • 4.1 Reagents and Water1
  • 4.2 Parallel Tests1
  • 4.3 Blank Test1
  • 4.4 Instruments and Equipment1
  • 4.5 Constant mass2
  • 5.Instruments and Equipment2
  • 6.Sample Preparation3
  • 6.1 Fibers and fiber products3
  • 6.2 Alumina Fiber Sol3
  • 7.Determination of loss on ignition3
  • 7.1 Principle3
  • 7.2 Test Procedure3
  • 7.3 Calculation of Results3
  • 8.Determination of silicon dioxide4
  • 8.1 Overview4
  • 8.2 Spectrophotometry4
  • 8.3 Gravimetric-Silica Molybdenum Blue Spectrophotometric Method5
  • 8.4 Potassium fluorosilicate titration method7
  • 9.1 Overview8
  • 9.2 EDTA complexation-zinc acetate back titration method8
  • 9.3 Precipitation Separation Method10
  • 9.4 Difference Subtraction11
  • 10 Determination of Boron Trioxide11
  • 10.1 Overview11
  • 10.2 Acid-Base Titration11
  • 10.3 Inductively Coupled Plasma Emission Spectrometry (ICP)12
  • 11 Determination of Zirconium Dioxide14
  • 11.1 Principle14
  • 11.2 Reagent14
  • 11.3 Test Procedure14
  • 11.4 Result Calculation14
  • 12.Silicon dioxide, aluminum oxide, calcium oxide, magnesium oxide, sodium oxide, potassium oxide, ferric oxide, titanium dioxide, phosphorus pentoxide, Determination of Zirconium Dioxide, Hafnium Dioxide, and Yttrium Trioxide - X-ray Fluorescence Spectrometry (XRF)15
  • 12.1 Principle15
  • 12.2 Reagent15
  • 12.3 Glass Sample Preparation16
  • 12.4 Preparation of standard glass samples, drift correction glass samples, and monitoring glass samples16
  • 12.5 Standard Working Curve Plotting16
  • 12.6 Drift Correction17
  • 12.7 Glass Sample Testing and Result Calculation17
  • 13 Zirconium dioxide, hafnium dioxide, yttrium oxide, calcium oxide, magnesium oxide, ferric oxide, titanium dioxide, lithium oxide, sodium oxide, Determination of potassium oxide, sulfur trioxide, and phosphorus pentoxide - Inductively coupled plasma atomic emission spectrometry (ICP)17
  • 13.1 Principle17
  • 13.2 Reagent18
  • 13.3 Preparation of test solution19
  • 13.4 Test Procedure19
  • 13.5 Result Calculation20
  • 14 Determination of Free Sodium21
  • 14.1 Principle21
  • 14.2 Reagent21
  • 14.3 Utensil Cleaning21
  • 14.4 Preparation of test solution21
  • 14.5 Test Procedure22
  • 14.6 Result Calculation22
  • 25 Appendix C (Informative) Calibration Curve26

Foreword

This document complies with the provisions of GB/T 1.1-2020 "Standardization Work Guidelines Part

1.Structure and Drafting Rules of Standardization Documents". Drafting. Please note that some content in this document may involve patents. The issuing organization of this document assumes no responsibility for identifying patents. This document was proposed by the China Building Materials Federation. This document is under the jurisdiction of the National Technical Committee on Standardization of Glass Fiber (SAC/TC245). This document was drafted by: Nanjing Guocai Testing Co., Ltd., a subsidiary of China National Testing & Inspection Holding Group, and the Aerospace Special Materials and Process Technology Research Institute. Shanghai Rongrong New Materials Technology Co., Ltd., Shandong Dongheng Guoxian New Materials Co., Ltd., Shandong Luyang Energy-Saving Materials Co., Ltd., Shandong Luko New Materials Co., Ltd., Anhui Yaoshi New Materials Technology Co., Ltd., Bruker (Beijing) Technology Co., Ltd., Jiangsu Qiyi Technology Limited Liability Company, Dezhou Shengyuan Fiber Technology Co., Ltd., China Chemical Fiber Industry Association, Shanghai Textile Research Institute Jiangban Textile Technology Service Co., Ltd. company. The main drafters of this document are. Li Yong, Wang Ling, Zhang Lei, Zhang Lijuan, Shi Zhuo, Guan Ketian, Song Jiandong, Pang Xiuxiu, Li Yang, Wang Ying, and Lü Liangyi. Ying Xiaohu, Wan Zetao, Zhu Chengzhuo, Wang Xinzong, Yang Jie, Gao Yumeng, Chen Yongjian, Li Deli, Wang Lili, Xu Liang, Lan Lin, Jiao Xiuling, Hao Zhengtao Qu Xiaoji. Chemical Analysis Methods for Alumina Fibers Warning

---Personnel using this document should have formal experience working in a chemical laboratory. This document does not cover all possible safety hazards. Problem. Users are responsible for taking appropriate safety and health measures and ensuring compliance with relevant national regulations.

1 Scope

GB/T 47093-2026 is the Chinese national standard covering the composition of alumina fibre - the alumina and silica proportions that decide its crystalline phase and its use temperature, and the alkali and iron impurities that lower both. It is the fibre of high-temperature furnace linings and of ceramic matrix composites. First edition, 19,000 words, published with GB/T 47086-2026 on fibre diameter. It was issued on 28 January 2026 and has been in force since 1 August 2026, as a first edition. The document is under the responsibility of the China Building Materials Federation. This page is published from the official record of the 2026 edition; the clause text of a standard this recent is not yet in circulation, and the figures, limits and tables it contains are those of the document itself, delivered in full with the English translation.

This document describes the method for analyzing the chemical composition of alumina fibers. This document applies to the determination of the chemical composition of alumina fibers, alumina fiber products, and alumina fiber sol.

2 Normative references

The contents of the following documents, through normative references within the text, constitute essential provisions of this document. Dated citations are not included. For references to documents, only the version corresponding to that date applies to this document; for undated references, the latest version (including all amendments) applies. This document.

GB/T 601 Preparation of Standard Titration Solutions for Chemical Reagents GB/T 4842 Argon

GB/T 6682 Specifications and test methods for water used in analytical laboratories

GB/T 8979 Pure Nitrogen, High-Purity Nitrogen and Ultra-Purity Nitrogen

GB/T 10067.44 Basic Technical Conditions for Electric Heating Devices - Part

44.Box-type Resistance Furnaces

GB/T 16597 General Rules for X-ray Fluorescence Spectrometry in Metallurgical Products

GB/T 18374 Terminology for Reinforcing Materials

GB/T 26810 Visible Spectrophotometer

3 Terms and Definitions

The terms and definitions defined in GB/T 18374 apply to this document.

4 General Rules

4.1 Reagents and Water Unless otherwise specified, all reagents used should be analytical grade, and reagents used to prepare standard stock solutions should be primary reference reagents or reagents with a purity greater than or equal to [a certain value]. 99.99%. The water used is of Grade I or higher as specified in GB/T 6682.

4.2 Parallel Tests Two experiments were conducted simultaneously under the same conditions.

4.3 Blank Test The test was conducted in parallel with the sample test, and the test procedures and conditions were completely consistent with the sample test, except that no sample was added.

4.4 Instruments and Equipment All equipment used should be inspected or calibrated regularly.

......
This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 30 pages — is available in the English PDF.

Referenced standards

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