GB/T 44538-2024Carbon based films - Determination of optical properties of amorphous carbon films by spectroscopic ellipsometry (English PDF)
碳基薄膜 椭偏光谱法测定非晶态碳基薄膜的光学性能
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Issued by
State Administration for Market Regulation, China National Standardization Administration
Level / Type
National · Recommended
Issue date
September 29, 2024
Implementation date
May 1, 2025
Scope
GB/T 44538-2024 is the English-translated version of 碳基薄膜 椭偏光谱法测定非晶态碳基薄膜的光学性能.
GB/T 44538-2024 — This paper describes the use of spectroscopic ellipsometry to determine the optical properties of amorphous carbon-based films (refractive index n and extinction coefficient k) and the use of n-k diagrams A method for classifying different types of amorphous carbon-based films by spectroscopy.
This document applies to non-metallic materials deposited by ion evaporation, sputtering, arc deposition, plasma-assisted chemical vapor deposition, hot wire, etc. Crystalline carbon-based films.
This document does not apply to amorphous carbon-based films modified by metals or silicon, or amorphous carbon with composition/property gradients through the film thickness. Base film.
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Document preview — GB/T 44538-2024
National Standard of the People's Republic of China
- ICS
- 25.220.99
- Classification
- A 29
Issued by: State Administration for Market Regulation, China National Standardization Administration
Contents
- Preface
- 1 Scope
- 2 Normative references
- 3 Terms and Definitions
- 4 Sample preparation
- 5 Equipment
- 5.1 Halogen lamp and blue LED lamp
- 5.2 Detector
- 5.3 Spectrometers connected to photomultiplier tubes (PMTs)/charge coupled devices (CCDs)/photodiode arrays (PDAs)
- 5.4 Software
- 5.5 Storage table
- 5.6 Goniometer
- 5.7 Camera
- 6 Test steps
- 6.1 Sample pretreatment
- 6.2 Experimental Preparation
- 6.3 Test conditions
- 6.4 Optical Model
- 6.5 Testing Process
- 6.6 Parallel tests
- 7 Classification of test results
- 8 Test report
- Appendix A (Normative) Classification method for optical properties of amorphous carbon-based films
Foreword
This document is in accordance with the provisions of GB/T 1.1-2020 "Guidelines for standardization work Part 1: Structure and drafting rules for standardization documents" Drafting is required.
This document modification adopts ISO 23216:2021 "Optical properties of amorphous carbon-based films by spectroscopic ellipsometry of carbon-based films".
This document has the following structural adjustments compared to ISO 23216:2021.
6.4 and 6.5 correspond to 6.4 in ISO 23216:2021; -6.6 corresponds to 6.5 in ISO 23216:2021.-the following editorial changes were made to this document.
Added the annotations of the types corresponding to each layer of the optical model in Figure 1; -Added title bar (see 5.1 to 5.7). -
1 Scope
This paper describes the use of spectroscopic ellipsometry to determine the optical properties of amorphous carbon-based films (refractive index n and extinction coefficient k) and the use of n-k diagrams A method for classifying different types of amorphous carbon-based films by spectroscopy.
This document applies to non-metallic materials deposited by ion evaporation, sputtering, arc deposition, plasma-assisted chemical vapor deposition, hot wire, etc.
Crystalline carbon-based films.
This document does not apply to amorphous carbon-based films modified by metals or silicon, or amorphous carbon with composition/property gradients through the film thickness.
Base film.
2 Normative references
This document has no normative references.
3 Terms and definitions
The following terms and definitions apply to this document.
Refractive index
The ratio of the speed of electromagnetic radiation in a vacuum to the speed of electromagnetic radiation in a medium.
Extinction coefficient the amount of electromagnetic radiation absorbed by a medium (matter).
4 Sample preparation
Amorphous carbon-based films on any substrate can be used for testing as long as the substrate is optically isotropic and has a usable optical model.
The test substrate is a mirror-finished silicon wafer. The mirror-finished silicon wafer can be used as a substrate for amorphous carbon films to meet different test requirements. The sample should be for uniform amorphous carbon-based films, the film thickness should be 0.02 µm~5 µm.
All relevant details of the sample should be provided, such as size, surface roughness, material type, composition, microstructure and processing process.
5 Equipment
5.1 Halogen lamp and blue LED lamp
Its spectral range should include 450 nm~950 nm.
5.2 Detector
Used to obtain ellipsometer measurement data, the spectral range should include 450 nm~950 nm.
......
This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 8 pages — is available in the English PDF.
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