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GB/T 44514-2024Micro-electromechanical system(MEMS) technology - Four-point bending test method for interfacial adhesion energy of layered MEMS materials (English PDF)

微机电系统(MEMS)技术 层状MEMS材料界面黏附能四点弯曲试验方法

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Issued by

State Administration for Market Regulation, China National Standardization Administration

Level / Type

National · Recommended

Issue date

September 29, 2024

Implementation date

September 29, 2024

Scope

GB/T 44514-2024 is the English-translated version of 微机电系统(MEMS)技术 层状MEMS材料界面黏附能四点弯曲试验方法.

GB/T 44514-2024 — This paper describes a four-point bending measurement method based on fracture mechanics concepts, using pure bending forces acting on layered MEMS materials.

The critical bending moment of the weakest interface steady-state cracking is used to measure the interface adhesion energy. This document applies to MEMS devices that deposit thin film layers on semiconductor substrates.

The total thickness of the thin film layer should be less than the supporting substrate (usually silicon 1/100 of the thickness of the wafer).

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Document preview — GB/T 44514-2024

National Standard of the People's Republic of China

ICS
31.080.99
Classification
L 59

Issued by: State Administration for Market Regulation, China National Standardization Administration

Contents

  • Preface
  • 1 Scope
  • 2 Normative references
  • 3 Terms, definitions, symbols and names
  • 3.1 Terms and Definitions
  • 3.2 Symbols and Names
  • 4 Test pieces
  • 4.1 General Requirements
  • 4.2 Shape of the test piece
  • 4.3 Dimensional Measurement
  • 4.4 Evaluation of energy release rate
  • 5 Test methods and test equipment
  • 5.1 Test Principle
  • 5.2 Test equipment
  • 5.3 Test Procedure
  • 5.4 Test environment
  • 6 Test Report
  • Appendix A (Informative) Failure modes in four-point bending test
  • A.1 General Principles
  • A.2 Failure Mode
  • References

Foreword

This document is in accordance with the provisions of GB/T 1.1-2020 "Guidelines for standardization work Part 1: Structure and drafting rules for standardization documents" Drafting is required.

This document is equivalent to IEC 62047-31:2019 "Semiconductor devices - Microelectromechanical devices - Part 31: Layered MEMS materials interface Four-point bending test method for surface bonding energy.

The following minimal editorial changes were made to this document.

To coordinate with the existing standards, the name of the standard is changed to "Microelectromechanical Systems (MEMS) Technology - Layered MEMS Material Interface Adhesion Four-point bending test method";

To show the original state of the test piece, Figure 1a) is added as a schematic diagram of the test piece with prefabricated cracks before the test, and a pressure roller is added.

and description of the support rollers.

1 Scope

This paper describes a four-point bending measurement method based on fracture mechanics concepts, using pure bending forces acting on layered MEMS materials.

The critical bending moment of the weakest interface steady-state cracking is used to measure the interface adhesion energy.

This document applies to MEMS devices that deposit thin film layers on semiconductor substrates. The total thickness of the thin film layer should be less than the supporting substrate (usually silicon 1/100 of the thickness of the wafer).

2 Normative references

This document has no normative references.

3 Terms, definitions, symbols and names

3.1 Terms and Definitions

The following terms and definitions apply to this document.

3.1.1

Energy release rate

The strain energy per unit surface area released during crack growth.

NOTE. The energy release rate is considered to be the crack driving force and is expressed in joules per square meter (J/m2).

3.1.2

interfacial adhesion energy the energy release rate when the interface crack starts to grow and expands steadily along the interface.

Note. Also known as critical energy release rate, its unit is joule per square meter (J/m2).

3.2 Symbols and names

The shape and symbol of the test piece are shown in Figure 1 and Table 1 respectively. The overall shape of the test piece is similar to a sandwich cantilever beam.

A prefabricated crack or a notch for crack initiation. After crack initiation, the crack extends along the weakest interface in the layered material system.

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This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 10 pages — is available in the English PDF.

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