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GB/T 44202-2024Sample preparation for testing aging degree of silk textile in museum collections (English PDF)

馆藏丝织品老化程度测试样品制备

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Issued by

SAMR; SAC

Level / Type

National · Recommended

Issue date

July 24, 2024

Implementation date

November 1, 2024

Scope

GB/T 44202-2024 is the English-translated version of 馆藏丝织品老化程度测试样品制备.

GB/T 44202-2024 is the Chinese national standard covering sample preparation for testing aging degree of silk textile in museum collections. Issued on 24 July 2024, it has been in force since 1 November 2024.

Document preview — GB/T 44202-2024

National Standard of the People's Republic of China

ICS
97.195
Classification
Y 04

Issued by: State Administration for Market Regulation; Standardization Administration of the PRC

Contents

  • Preface...
  • 1 Scope...
  • 2 Normative referenced documents...
  • 3 Terms and Definitions...
  • 4 Sampling...
  • 4.1 Sampling plan...
  • 4.2 Sampling Process...
  • 5 Sample processing...
  • 5.1 Sample Cleaning...
  • 5.2 Sample Humidity Conditioning...
  • 6 Sample preparation...
  • 7 Sample Information Registration...
  • Appendix A (Informative) Sample Record Sheet for Sampling Information of Silk Textiles in the Collection...
  • Appendix B (Informative) Sample Information Sheet for Silk Fabric Aging Degree Test in Collections... References...

Foreword

This document is in accordance with the provisions of GB/T 1.1-2020 "Guidelines for standardization work Part 1: Structure and drafting rules for standardization documents" Drafting.

Please note that some of the contents of this document may involve patents. The issuing organization of this document does not assume the responsibility for identifying patents.

This document is proposed by the State Administration of Cultural Heritage of the People's Republic of China.

This document is under the jurisdiction of the National Technical Committee for Cultural Relics Protection Standardization (SAC/TC 289).

This document was drafted by: University of Science and Technology of China, National Museum of China, Fujian University of Technology, Beijing Zhongke Standard Technology Group Limited company.

The main drafters of this document are: Gong Yuxuan, Gong Decai, Tie Fude, Wang Zhimin, Cheng Weizhi, Zhou Guangzhao, Qiao Chengquan, Hu Shuangqing, Zhong Bochao, Zhang Xiaoning, Wang Kai, Luo Xianjuan.

Sample preparation for testing the aging degree of silk fabrics in museum collections

1 Scope

This document specifies the requirements for sampling, processing, preparation, and sample information registration for testing the degree of aging of silk textiles in collections.

This document is applicable to amino acid analysis, scanning electron microscopy, thermogravimetric analysis, Fourier transform infrared spectroscopy, etc.

Sample preparation for external spectroscopy and X-ray powder diffraction test methods.

2 Normative references

GB/T 6529-2008

GB/T 13464-2008

GB/T 23863-2009

GB/T 32016-2015

3 Terms and definitions

The terms and definitions defined in GB/T 6529-2008 and the following apply to this document.

3.1 Aging degree of silk textile

The level of changes in microstructure and macroscopic properties of damaged silk fabrics in museum collections compared to fresh silk.

4 Sampling

4.1 Sampling plan

The preparation of samples for testing the aging degree of silk fabrics in museums (hereinafter referred to as “samples”, including samples to be tested and reference samples1)) should be the same as that of the cultural relics.

The responsible units shall formulate a sampling plan based on the sampling purpose after consultation. The relevant requirements of the sampling plan are as follows.

The impact of the materials and processes used in previous protection and restoration on the test should be fully considered; a) Determine the sampling location, number of samples, and amount of samples according to the needs and the characteristics of the cultural relics, such as grade, preservation status, disease, and organizational structure.

(such as sample size, sample area and sample mass), sampling method, sample packaging and preservation method, etc.;

b) Priority should be given to sampling from the remaining pieces (fragments) or places that have little impact on the value of cultural relics (such as patterns, designs, etc.); c) Determine the disposal method of the remaining samples after the sample testing (such as returning them to the responsible unit of the cultural relics, retaining them, etc.). d)

4.2 Sampling process

The sampling process is carried out according to the sampling plan.

— ---

1) Reference samples are new samples used for analysis and comparison, which are prepared, manufactured and tested in the same way as the samples to be tested.

......
This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 15 pages — is available in the English PDF.

Referenced standards

Editions of GB/T 44202

EditionTitleRevisionStatus
GB/T 44202-2024Sample preparation for testing aging degree of silk textile in museum collectionscurrent editionCurrent

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