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GB/T 40933-2021Plastics - Film and sheeting - Guidance on the testing of thermoplastic films (English PDF)

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Issued by

SAMR; SAC

Level / Type

National · Recommended

Issue date

November 26, 2021

Implementation date

June 1, 2022

Scope

GB/T 40933-2021 (Plastics - Film and sheeting - Guidance on the testing of thermoplastic films) is available as an English-translated PDF.

GB/T 40933-2021 — This document gives producers and users test procedures for selecting and characterizing single or multilayer thermoplastic films. The purpose is to provide guidance for testing of films for which there are no existing standards or specifications. NOTE: This document does not cover sample preparation. This document is intended to provide general guidance. If a standard exists for a particular film product, the requirements of that document take precedence over this document. It does not involve specific application-specific requirements stipulated by a country, region, or industry. The importance and suitability of the data is determined by the user.

Document preview — GB/T 40933-2021

National Standard of the People's Republic of China

Issued by: SAMR; SAC

Contents

  • Foreword3
  • Introduction4
  • 1 Scope5
  • 2 Normative references5
  • 3 Terms and definitions8
  • 4 Sample preparation and state conditioning8
  • 5 Test requirements9
  • 6 Result report9
  • Annex NA (informative) Correspondence between Chinese documents and international documents normatively cited in this document13
  • Bibliography15

1 Scope

This document gives producers and users test procedures for selecting and characterizing single or multilayer thermoplastic films. The purpose is to provide guidance for testing of films for which there are no existing standards or specifications.

NOTE: This document does not cover sample preparation.

This document is intended to provide general guidance. If a standard exists for a particular film product, the requirements of that document take precedence over this document. It does not involve specific application-specific requirements stipulated by a country, region, or industry.

The importance and suitability of the data is determined by the user.

2 Normative references

The following referenced documents are indispensable for the application of this document. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies.

ISO 307, Plastics - Polyamides - Determination of viscosity number

ISO 527-3, Plastics - Determination of tensile properties - Part 3: Test conditions for films and sheets

ISO 1133-1, Plastics - Determination of the melt mass-flowrate (MFR) and melt volume-flow rate (MVR) of thermoplastics - Part 1: Standard method

ISO 1183-1, Plastics - Methods for determining the density of non-cellular plastics - Part 1: Immersion method, liquid pycnometer method and titration method

ISO 1183-2, Plastics - Methods for determining the density of non-cellular plastics - Part 2: Density gradient column method

ISO 1183-3, Plastics - Methods for determining the density of non-cellular plastics - Part 3: Gas pyknometer method

ISO 2813, Paints and varnishes - Determination of specular gloss of non-metallic paint film at 20°,60° and 85°

ISO 4589-1, Plastics - Determination of burning behaviour by oxygen index - Part 1: Guidance

ISO 4589-2, Plastics - Determination of burning behaviour by oxygen index - Part 2: Ambient-temperature test

ISO 4592, Plastics - Film and sheeting - Determination of length and width

ISO 4593, Plastics - Film and sheeting - Determination of thickness by mechanical scanning

ISO 6383-1, Plastics - Film and sheeting - Determination of tear resistance - Part 1: Trouser tear method

ISO 6383-2, Plastics - Film and sheeting - Determination of tear resistance - Part 2: Elmendorf method

ISO 7765-1, Plastics - Film and sheeting - Determination of impact resistance by the free-falling dart method - Part 1: Staircase methods

ISO 7765-2, Plastics film and sheeting - Determination of impact resistance by the free-falling dart method - Part 2: Instrumented puncture test

ISO 8256, Plastics - Determination of tensile-impact strength

ISO 8295, Plastics - Film and sheeting - Determination of the coefficients of friction

ISO 8296, Plastics - Film and sheeting - Determination of wetting tension

ISO 9773, Plastics - Determination of burning behaviour of thin flexible vertical specimens in contact with a small-flame ignition source

ISO 11357-2, Plastics - Differential scanning calorimetry (DSC) - Part 2:

Determination of glass transition temperature

ISO 11357-3, Plastics - Differential scanning calorimetry (DSC) - Part 3:

Determination of temperature and enthalpy of melting and crystallization

ISO 11443, Plastics - Determination of the fluidity of plastics using capillary and slit-die rheometers Permanent Deformation and Stress Retention of Stretch Wrap Film

ASTM D 5748, Standard Test Method for Protrusion Puncture Resistance of Stretch Wrap Film

ASTM F 88, Standard Test Method for Seal Strength of Flexible Barrier Materials

ASTM F 1921, Standard Test Methods for Hot Seal Strength (Hot Tack) of Thermoplastic Polymers and Blends Comprising the Sealing Surfaces of Flexible Webs

3 Terms and definitions

For the purposes of this document, the following terms and definitions apply.

3.1 film

Sheets with a nominal thickness not greater than 0.25mm.

NOTE 1: Although ISO 472 does not clearly stipulate, it mentions the limit of the nominal thickness of the film to 0.25mm. ASTM D883 clearly stipulates that the nominal thickness of the film is <=0.25mm.

NOTE 2: Since the sheet with a nominal thickness greater than 0.25mm is too rigid, it is not suitable for the test method for testing thinner films.

4 Sample preparation and state conditioning

4.1 Polymer properties

Many polymer properties are related to the processability and yield of products, so they are concerned by producers and users of film products. These properties include density, flow characteristics and thermal properties.

The above properties shall follow the sample preparation and state conditioning requirements specified in the material standard. If there is no material standard, the requirements specified in this document shall be followed.

4.2 Sample preparation

This document does not contain standards for film preparation. Table 1 describes the preparation methods of some common films of different materials and structures.

Table 1 -- Typical preparation methods for producing plastic films

Cold roll casting Sink chilling Blow molding - standard Blow molding - blowing up and cooling Blow molding - blowing down and cooling Stretching method (biaxially stretching film)

Double bubble method (biaxially stretching film)

Calendering The films used for testing and characterization shall be produced in accordance with the requirements of the corresponding product standards. If a product standard does not exist or does not address film fabrication, the same basic process as for commercial application of films shall be used. Typical processing conditions shall be used. The specific process, equipment and materials used are optimized. No device or technique shall be employed which would not be used during accepted manufacturing practice. If special conditions or equipment are used, it shall be indicated in the test report.

Key process variables shall be recorded. Keep records for a reasonable period of time for future reference in the event of a dispute or disagreement.

4.3 Sample state conditioning

For the properties described in Table 2, the preparation and conditioning requirements specified in the material or product standard shall apply. In the absence of material standards or product standards, the requirements specified in this document shall be followed.

5 Test requirements

In the absence of material or product standards, the test methods, test conditions and units specified in Table 2 shall be used when determining the data. The number of specimens shall be determined according to the requirements of specific test standards.

All tests in Table 2 need not be performed in every case. The specific test part depends on the film type, intended use and test objectives. That is, research and development, manufacturing, quality control, may be negotiated by the relevant parties.

6 Result report

The type of film suitable for testing, its use and any agreement between the supplier and the purchaser, the report shall normally include the following. In addition, any other information and data of a non-proprietary nature considered suitable for the intended purpose of the test shall be included:

a) Description of the film, for example, type, material, formulation components (if it is a blended material), structure (if it is co-extruded or compounded);

......
This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — all pages — is available in the English PDF.

Referenced standards

Normative references

ISO 307 · ISO 527 · ISO 1133 · ISO 1183 · ISO 2813 · ISO 4589 · ISO 4592 · ISO 4593 · ISO 6383 · ISO 7765 · ISO 8256 · ISO 8295 · ISO 8296 · ISO 9773 · ISO 11357 · ISO 11443

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