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GB/T 40311-2021Vanadium slag—Determination of multi-element contents—Wavelength dispersive X-ray fluorescence spectrometry(fused cast bead method) (English PDF)

钒渣 多元素的测定 波长色散X射线荧光光谱法(熔铸玻璃片法)

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Issued by

SAMR; SAC

Level / Type

National · Recommended

Issue date

August 20, 2021

Implementation date

March 1, 2022

Scope

GB/T 40311-2021 is the English-translated version of 钒渣 多元素的测定 波长色散X射线荧光光谱法(熔铸玻璃片法).

GB/T 40311-2021 describes how to measure several components of vanadium slag at once by wavelength dispersive X-ray fluorescence spectrometry, with the sample fused into a cast glass bead.

The method determines silica, aluminium oxide, calcium oxide, magnesium oxide, manganese oxide, vanadium pentoxide, titanium dioxide, chromium trioxide, phosphorus and total iron, each within the measuring range given in a table, from 0.010 to 0.60 for phosphorus up to 20.0 to 45.0 for total iron.

It relies on the general rules for XRF analysis of metallurgical products, on GB/T 6379 for accuracy and precision and on YB/T 008 for the slag itself. Steelworks and vanadium plant laboratories use it. It was issued on 20 August 2021 and has applied since 1 March 2022.

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Document preview — GB/T 40311-2021

National Standard of the People's Republic of China

ICS
77.100
Classification
H 11

Issued by: State Administration for Market Regulation; Standardization Administration of the PRC

Contents

  • Foreword
  • 1 Scope
  • 2 Normative references

Foreword

This document is in accordance with the provisions of GB/T 1.1-2020 "Guidelines for Standardization Work Part 1: Structure and Drafting Rules of Standardization Documents" Drafting.

1 Scope

This document describes the use of wavelength dispersive X-ray fluorescence spectrometry (fused-cast glass sheet method) to determine silica, aluminum oxide, The content of calcium oxide, magnesium oxide, manganese oxide, vanadium pentoxide, titanium dioxide, chromium trioxide, phosphorus and total iron.

This document is applicable to the determination of multiple elements in vanadium slag. The measurement range of each element (mostly calculated as oxide) is shown in Table 1.

2 Normative references

The contents of the following documents constitute the indispensable clauses of this document through normative references in the text. Among them, dated quotations Only the version corresponding to that date is applicable to this document; for undated reference documents, the latest version (including all amendments) is applicable to this document.

GB/T 6379.1 Accuracy of measurement methods and results (accuracy and precision) Part 1: General principles and definitions

GB/T 6379.2 Accuracy of measurement methods and results (accuracy and precision) Part 2: Determine the repeatability of standard measurement methods Basic methods of sex and reproducibility

GB/T 6682 Analytical laboratory water specifications and test methods

GB/T 8170 Numerical rounding rules and the expression and determination of limit values

GB/T 16597 General Rules of X-ray Fluorescence Spectrometry for Analysis Methods of Metallurgical Products

YB/T 008 Vanadium slag

......
This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 17 pages — is available in the English PDF.

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