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GB/T 40281-2021Determination of content of nonmetallic inclusions in steel—Extremum analytical method (English PDF)

钢中非金属夹杂物含量的测定 极值分析法

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Issued by

SAMR; SAC

Level / Type

National · Recommended

Issue date

August 20, 2021

Implementation date

March 1, 2022

Scope

GB/T 40281-2021 is the English-translated version of 钢中非金属夹杂物含量的测定 极值分析法.

GB/T 40281-2021 sets out the extreme value analysis method for the largest non-metallic inclusions in steel.

Instead of rating inclusions against charts, as GB/T 10561 does, it measures the largest inclusion in each of many inspection areas and fits the data to a Gumbel extreme value distribution, so that results are continuously comparable and can be related to the life of parts.

It covers sample preparation, inclusion inspection, calculation of the extreme values, drawing of the extreme value graph, data validity analysis, evaluation of differences and the test report.

It applies to steel, steel ingots and continuously cast slabs and can be used for other microstructural features, but not for exogenous inclusions. It was issued on 20 August 2021 and has applied since 1 March 2022.

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Document preview — GB/T 40281-2021

National Standard of the People's Republic of China

ICS
77.040.99
Classification
H 24

Issued by: State Administration for Market Regulation; Standardization Administration of the PRC

Contents

  • Foreword
  • Introduction
  • 1 Scope
  • 2 Normative references
  • 3 Terms and definitions
  • 4 Symbols and abbreviations
  • 5 Principle and Application
  • 6 Operation process
  • 7 Test report
  • Appendix A (informative) Calculation formula for extreme value of non-metallic inclusion size (length, diameter or area)
  • Appendix B (informative) Example of extreme value analysis of non-metallic inclusions in steel
  • Appendix C (Informative) Example of extreme value analysis of non-metallic inclusions in the as-cast state of the smelting process

Foreword

This document is in accordance with the provisions of GB/T 1.1-2020 "Guidelines for Standardization Work Part 1: Structure and Drafting Rules of Standardization Documents" Drafting.

Introduction

The presence of large non-metallic oxide inclusions in steel will cause the decline of the metal's mechanical properties, resulting in unqualified performance. Non-metallic inclusions The test method standards such as GB/T 10561 adopt the comparative method to assess the level. The level and the length of non-metallic inclusions increase exponentially.

Continuous data is difficult to correlate with the fatigue life of parts, and the detected non-metallic inclusions are accidental and the data is discrete. Some research sheets Obviously, the extreme value analysis method applies statistical principles, increases the number of inspections for non-metallic inclusions, and performs statistical analysis on the data, which can be reflected to the greatest extent.

Reflect the distribution of non-metallic inclusions and reduce chance. The extreme value of non-metallic inclusions analyzed by the extreme value analysis method can better reflect the The overall state of the existing non-metallic inclusions is continuously comparable in value, which can establish a correlation with the life of the part.

The extreme value analysis method allows the tester to analyze the maximum value of the endogenous non-metallic inclusions or the second phase in the steel. Under normal circumstances, measurable The largest oxidized inclusion in the tapped sample. If necessary, the maximum value of multiple types of inclusions can also be determined.

Measure the maximum value of oxides, sulfides, silicates, point-shaped non-metallic inclusions, titanium carbonitride and other inclusions. Extreme value analysis method is also available It is used to determine the characteristics of other microstructures, such as the extreme value of the graphite ball size in ductile cast iron, and the maximum value of carbides in tool steel and bearing steel. Large particle size and maximum diameter of crystal grains.

The distribution characteristics of foreign inclusions in steel are not easy to predict, and other non-destructive testing methods, such as ultrasonic flaw detection, should be used to determine.

1 Scope

This document specifies the sample preparation, inclusion inspection, extreme value calculation, extreme value graph drawing, and data for the extreme value analysis method of non-metallic inclusions in steel Effectiveness analysis, difference evaluation and test report, etc.

This document is applicable to the extreme value analysis of non-metallic inclusions in steel, steel ingots and continuous casting slabs. The characteristic values of other microstructures can also be referred to use. This document is not applicable to the extreme value analysis of foreign non-metallic inclusions.

2 Normative references

The contents of the following documents constitute the indispensable clauses of this document through normative references in the text. Among them, dated quotations Only the version corresponding to that date is applicable to this document; for undated reference documents, the latest version (including all amendments) is applicable to this document.

GB/T 10561 Standard Determination of Non-metallic Inclusions in Steel Grading Chart Microscopic Inspection Method

GB/T 13298 Metal Microstructure Inspection Method

GB/T 30067 Metallographic Terms

3 Terms and definitions

The following terms and definitions defined in GB/T 30067 apply to this document.

3.1 Extreme value distribution

The probability density function of the characteristic value x of the largest inclusion measured on a specific area or volume meets the formula (1), then a continuous random variable x has a maximum distribution of binary parameters (Gumbel). […]

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This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 21 pages — is available in the English PDF.

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