GB/T 35151-2017Determination of total organic carbon in limestone (English PDF)
石灰石中总有机碳的测定方法
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Issued by
SAMR; SAC
Level / Type
National · Recommended
Issue date
December 29, 2017
Implementation date
November 1, 2018
Scope
GB/T 35151-2017 is the English-translated version of 石灰石中总有机碳的测定方法.
GB/T 35151-2017 is the Chinese standard "Determination of total organic carbon in limestone". Its scope clause reads: This standard specifies the three methods of quantitative determination of total organic carbon in limestone.
This standard applies to the determination of total organic carbon in calcareous materials such as limestone. Its clauses include test the basic requirements; reagents and materials.
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Document preview — GB/T 35151-2017
National Standard of the People's Republic of China
- ICS
- 91.100.10
- Classification
- Q 11
Issued by: State Administration for Market Regulation; Standardization Administration of the PRC
Contents
- Preface
- 1 Scope
- 2 Normative references
- 3 test the basic requirements
- 4 Reagents and materials
- 5 instruments and equipment
- 7 Wet Oxidation --- Gravimetric Analysis (Standard Method)
- 8 high temperature furnace oxidation --- gravimetric method (alternative method)
- 9 high temperature furnace oxidation --- Infrared Analysis (alternative method)
- 10 Repeatability and reproducibility limits
1 Scope
This standard specifies the three methods of quantitative determination of total organic carbon in limestone.
This standard applies to the determination of total organic carbon in calcareous materials such as limestone.
2 Normative references
The following documents for the application of this document is essential. For dated references, only the dated version applies to this article
Pieces. For undated references, the latest edition (including all amendments) applies to this document.
GB/T 2007.1 bulk mineral products sampling, sample preparation General manual sampling method
GB/T 6682 analytical laboratory water specifications and test methods
3 test the basic requirements
3.1 The number of tests and requirements
The number of tests for each test is defined as two and the absolute difference between the two tests is within the limit of repeatability (see Chapter 10)
The average of the results indicates the measurement result.
3.2 Quality and result representation
Mass units with "grams (g)", accurate to 0.0001g.
Unless otherwise stated, the analytical results are expressed in% by mass and the analytical results are expressed in% to two decimal places.
3.3 blank test
The test results obtained were corrected by not adding the test sample, following the same analytical procedure and using the same reagent amount.
4 Reagents and materials
4.1 General
Reagents used should be no lower than analytical grade, unless otherwise stated. The reagent used for calibration should be the reference reagent. The water used should not be less than
GB/T 6682 provisions of the three water requirements.
The density of commercially available concentrated liquid reagents listed in this standard refers to the density (rho) of 20 ° C in grams per cubic centimeter (g/cm3).
In chemical analysis, the acid used, who did not note concentration refers to the commercially available concentrated acid.
Reagent dilution is expressed in terms of volume ratio, for example, hydrochloric acid (1 2) indicates that 1 part by volume of concentrated hydrochloric acid is mixed with 2 parts by volume of water.
4.2 Hydrochloric acid (HCl)
1.18g/cm3 ~ 1.19g/cm3, the mass fraction of 36% to 38%.
......
This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 15 pages — is available in the English PDF.
Referenced standards
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