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GB/T 34698-2017Rubber compounding ingredients - Determination of water soluble substance of silica, precipitated, hydrated - Electrolytic conductivity method (English PDF)

橡胶配合剂 沉淀水合二氧化硅水可溶物含量的测定 电导率法

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Issued by

SAMR; SAC

Level / Type

National · Recommended

Issue date

November 1, 2017

Implementation date

May 1, 2018

Scope

GB/T 34698-2017 is the English-translated version of 橡胶配合剂 沉淀水合二氧化硅水可溶物含量的测定 电导率法.

GB/T 34698-2017 is the Chinese standard "Rubber compounding ingredients - Determination of water soluble substance of silica, precipitated, hydrated - Electrolytic conductivity method".

Its scope clause reads: This standard specifies the method for the determination of the water-soluble content of precipitated hydrated silica by the conductivity method.

This standard applies to sulfuric acid precipitation produced hydrated silica. Other methods to produce precipitated hydrated silica can be used for reference. Its clauses include principle; reagents and materials; instruments.

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Document preview — GB/T 34698-2017

National Standard of the People's Republic of China

ICS
83.040.20
Classification
G 49

Issued by: State Administration for Market Regulation; Standardization Administration of the PRC

Contents

  • 1 Scope
  • 2 Normative references
  • 3 principle
  • 4 Reagents and materials
  • 5 instruments

1 Scope

This standard specifies the method for the determination of the water-soluble content of precipitated hydrated silica by the conductivity method.

This standard applies to sulfuric acid precipitation produced hydrated silica. Other methods to produce precipitated hydrated silica can be used for reference.

2 Normative references

The following documents for the application of this document is essential. For dated references, only the dated version applies to this article

Pieces. For undated references, the latest edition (including all amendments) applies to this document.

GB/T 6003.1 Test sieves - Technical requirements and testing - Part 1. Wire mesh sieve test sieves

GB/T 8170 rounded repair rules and limit values of the representation and judgment

HG/T 3061 rubber compound precipitated hydrated silica

3 principle

The conductivity of the solution is the ability of the anions and cations to migrate between positive and negative electrodes, and the conductivity is proportional to the concentration of ions in solution

For example, the conductivity can be indirectly measured by measuring the content of soluble salts.

4 Reagents and materials

Unless otherwise noted, use only the following reagents and materials in the assay.

--- Sodium sulfate (Na2SO4), analytical grade;

--- Distilled or deionized water or rather pure water.

5 instruments

5.1

Analytical balance, dividing the value of 0.1mg.

5.2

Mortar.

5.3

magnetic stirrer.

5.4

Conductivity meter, with a constant 1.0cm-1 conductivity electrode.

5.5

stoppered conical flask, 250mL.

5.6

test sieve, Phi200mm × 25mm/0.25mm, in line with the provisions of GB/T 6003.1.

5.7

measuring cylinder, 250mL.

5.8

magnetic stirring rod, the surface of PTFE or fluorocarbon chemical resistant coating, the size suitable for 250mL stopper […]

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This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 15 pages — is available in the English PDF.

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