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GB/T 32263-2015Highly purified compound—Reagent for pesticide residue analysis—Method of the (English PDF)

高纯化合物 农残分析用化合物的测定 气相色谱-电子捕获检测器(ECD)法

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Issued by

SAMR; SAC

Level / Type

National · Recommended

Issue date

December 10, 2015

Implementation date

January 1, 2017

Scope

GB/T 32263-2015 is the English-translated version of 高纯化合物 农残分析用化合物的测定 气相色谱-电子捕获检测器(ECD)法.

GB/T 32263-2015 is the Chinese standard "Highly purified compound—Reagent for pesticide residue analysis—Method of the". Its scope clause reads: This standard specifies the gas chromatography - electron capture detector (ECD) compound pesticide residue analysis method for determination.

This standard applies to the determination of pesticide residues and other halogen negative electrical characteristics of strong indicators of high-purity solvents contained.

Its clauses include terms and definitions; principle of the method; reagents and materials.

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Document preview — GB/T 32263-2015

National Standard of the People's Republic of China

ICS
71.040
Classification
N 04

Issued by: State Administration for Market Regulation; Standardization Administration of the PRC

Contents

  • 1 Scope
  • 2 Normative references
  • 3 Terms and Definitions
  • 4 principle of the method
  • 5 Reagents and materials

1 Scope

This standard specifies the gas chromatography - electron capture detector (ECD) compound pesticide residue analysis method for determination.

This standard applies to the determination of pesticide residues and other halogen negative electrical characteristics of strong indicators of high-purity solvents contained.

2 Normative references

The following documents for the application of this document is essential. For dated references, only the dated version suitable for use herein

Member. For undated references, the latest edition (including any amendments) applies to this document.

GB/T 4946 GC term

GB/T 9722 General chemical reagent gas chromatography

GB/T 14666 analytical chemistry terms

JJG700-1999 gas chromatograph

3 Terms and Definitions

GB/T 4946, GB/T 9722, GB/T 14666 and defined by the following terms and definitions apply to this document.

3.1 Pesticide residue analysis compound

Pesticide grade reagents pesticidegradesolvent

Suitable for Pesticide Residue Analysis as a reagent solvent.

3.2 Concentration factor

Analytes through methods such as rotary evaporation concentrated volume ratio of volume and concentration before concentration after.

4 principle of the method

Electron capture detector is an ionization detector, with high selectivity and sensitivity, only for substances with a negative electrical properties, such as those containing

Halogen, sulfur, phosphorus, nitrogen substances responding. Pesticide residues pesticide content analysis of key features compound index. Traces of pesticide residues

After concentrated by gas chromatography - electron capture detector was used to detect, and the chromatograms corresponding data record by a data processing system.

5 Reagents and materials

5.1 Reagents

Hexane. pesticide grade.

......
This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 15 pages — is available in the English PDF.

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