GB/T 26930.5-2011Carbonaceous materials for the production of primary aluminium -- Pitch for electrodes -- Part 5: Determination of content of toluene-insoluble material (English PDF)
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Issued by
General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China
Level / Type
National · Recommended
Issue date
September 29, 2011
Implementation date
May 1, 2012
Scope
GB/T 26930.5-2011 (Carbonaceous materials for the production of primary aluminium -- Pitch for electrodes -- Part 5: Determination of content of toluene-insoluble material) is available as an English-translated PDF.
GB/T 26930.5-2011 — This section GB/T 26930 specifies the method for determination of bituminous coal for the production of primary aluminum in toluene insolubles content. This section applies to the determination of primary aluminum production of coal pitch toluene insolubles content. NOTE. The content of toluene-insoluble matter generally refers to the so-called "resin alpha beta sum."
Document preview — GB/T 26930.5-2011
National Standard of the People's Republic of China
- ICS
- 71.100.10
- Classification
- Q 52
Issued by: General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China
Contents
- Foreword
- 1 Scope
- 2 Normative references
- 3 PRINCIPLE OF THE METHOD
- 4 Reagents
- 4.1 Toluene. AR.
- 4.2 acetone. AR.
- 5 Instruments
- 5.1 Erlenmeyer flask. volume 500mL, made of silicon borate glass, frosted glass interface.
- 5.4 Oven. Can temperature at 105 degrees C ~ 110 degrees C.
- 6 sample preparation
Foreword
GB/T 26930 "carbonaceous materials used in aluminum production bituminous coal" There are five sections.
--- Part 1. Determination of moisture content - Azeotropic distillation method;
--- Part 2. Determination of softening point and ball method;
--- Part 3. Determination of density Pyknometer;
--- Part 4. Determination of quinoline insoluble content;
--- Part 5. Determination of toluene-insoluble matter content.
This is Part 5.
This section drafted in accordance with GB/T 1.1-2009 given rules.
This section uses the translation method identical with ISO 6376. 1980 "carbonaceous materials used in aluminum production bituminous coal toluene insolubles content
Determination. " This part identical with ISO 6376. 1980, the deleted its preamble.
Consistency correspondence between this part of international documents and normative references of our files are as follows.
--- GB/T 26297.5 carbonaceous materials used in aluminum sampling method - Part 5. coal tar pitch (ISO 6257.2002, MOD).
This section is responsible for drafting unit. Cable-Development Co., Ltd., China Nonferrous Metals Industry Standards Metrology and Quality Institute, Aluminum Corporation of China
Ltd. Zhengzhou Research Institute.
Participated in the drafting of this section. Beijing Science and Technology Co., Ltd. British Spike.
1 Scope
This section GB/T 26930 specifies the method for determination of bituminous coal for the production of primary aluminum in toluene insolubles content.
This section applies to the determination of primary aluminum production of coal pitch toluene insolubles content.
NOTE. The content of toluene-insoluble matter generally refers to the so-called "resin alpha beta sum."
2 Normative references
The following documents for the application of this document is essential. For dated references, only the dated version suitable for use herein
Member, undated references, the latest edition (including any amendments) applies to this document.
ISO 6257 carbonaceous materials used in aluminum bituminous coal sampling method (Carbonaceousmaterialsusedintheproductionof
aluminium-Pitchforelectrodes-Sampling)
3 PRINCIPLE OF THE METHOD
And provisions within the period prescribed temperature, a sample was dissolved with toluene, extract the toluene insolubles, filtered and weighed amount of residue, thereby meter
The content of toluene-insoluble matter is calculated.
4 Reagents
4.1 Toluene. AR.
4.2 acetone. AR.
5 Instruments
5.1 Erlenmeyer flask. volume 500mL, made of silicon borate glass, frosted glass interface.
Reflux condenser 5.2. Effective length 300mm, bottom frosted glass cone, can be fixed in the conical flask (5.1) interface.
5.3 Filter crucible. glass, volume of about 30mL. The bottom is a porosity of 10µm ~ 16µm sintered glass disc, the main dimensions
As follows. disc diameter. 30mm; height (upper edge of the disc to the ring). 35mm.
5.4 Oven. Can temperature at 105 degrees C ~ 110 degrees C.
6 sample preparation
Sampling in accordance with ISO 6257. On solid asphalt, crushed sample to make it through the sieve of 500µm aperture sieve. Of liquid asphalt, so
To take samples.
......
This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — all pages — is available in the English PDF.
Referenced standards
Normative references
ISO 6257
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Related Standards
GB/T 26930.1-2011 — Carbonaceous materials for the production of primary aluminium -- Pitch for electrodes -- Part 1: Determination of water content -- Azeotropic distillation (Dean and Stark) method
GB/T 26930.10-2014 — Carbonaceous materials used in the production of aluminium - Pitch for electrodes - Part 10: Determination of sulfur content by an instrumental method
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