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GB/T 26085-2010Test method and determination of total tin in antifouling paints for ship (English PDF)

船舶防污漆锡总量的测试及判定

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Issued by

SAMR; SAC

Level / Type

National · Recommended

Issue date

January 10, 2011

Implementation date

July 1, 2011

Scope

GB/T 26085-2010 is the English-translated version of 船舶防污漆锡总量的测试及判定.

GB/T 26085-2010 is the Chinese standard "Test method and determination of total tin in antifouling paints for ship".

Its scope clause reads: This standard specifies the determination by graphite furnace atomic absorption spectrometry (GFAAS) the total amount of antifouling paint tin reagents, equipment, Sampling, test procedures, and the results of the calculation result judgment and so on.

This standard applies to the determination of the total amount of antifouling paint tin, also applies to the identification of organotin compounds as a biocide in anti-ship Dirty paint. Its clauses include fundamentals; reagents.

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Document preview — GB/T 26085-2010

National Standard of the People's Republic of China

ICS
47.020.05
Classification
U 05

Issued by: State Administration for Market Regulation; Standardization Administration of the PRC

Contents

  • 1 Scope
  • 2 Normative references
  • 3 Fundamentals
  • 4 Reagents

1 Scope

This standard specifies the determination by graphite furnace atomic absorption spectrometry (GFAAS) the total amount of antifouling paint tin reagents, equipment,

Sampling, test procedures, and the results of the calculation result judgment and so on.

This standard applies to the determination of the total amount of antifouling paint tin, also applies to the identification of organotin compounds as a biocide in anti-ship

Dirty paint.

2 Normative references

The following documents contain provisions which, through reference in this standard and become the standard terms. For dated references, subsequent

Amendments (not including errata content) or revisions do not apply to this standard, however, encourage the parties to the agreement are based on research

Whether the latest versions of these documents. For undated reference documents, the latest versions apply to this standard.

GB/T 1725-2007 Paints, varnishes and plastics - Determination of volatile matter content is not (ISO 3251.2003, IDT)

GB/T 3186 Paints, varnishes and raw materials for paints and varnishes - Sampling (GB/T 3186-2006, ISO 15528.2000, IDT)

GB/T 6682-2008 analytical laboratory use specifications and test methods (ISO 3696. 1987, MOD)

GB/T 6822-2007 rust hull antifouling system

JJG694 atomic absorption spectrophotometer

3 Fundamentals

The antifouling paint dry sample with a suitable acid solution was sealed microwave digestion, the rush acid, the volume was treated as ascorbic acid group

Modifiers, effective use of the existing graphite furnace atomic absorption spectrometry (GFAAS) or to meet the precision [inductively coupled plasma

Emission Spectrometry/Mass Spectrometry (ICP/MS), X fluorescence spectrometry (XRF) and inductively coupled plasma atomic emission spectrometry (ICP-AES), etc.] measured

The concentration of a given sample of tin. Then, based on a simple formula can calculate the tin content in the sample.

4 Reagents

4.1

hydrochloride (rho~1.19g/mL).

Nitrate 4.2 (rho~1.42g/mL).

4.3

sulfate (rho~1.98g/mL).

4.4

for the two test water or distilled water GB/T 6682-2008 requirements.

4.5 volume fraction of 10% hydrochloric acid solution

with hydrochloric acid (4.1) and a volume ratio of distilled water was prepared 1.9 ratio of volume fraction of 10%

Hydrochloric acid solution.

Completely dissolved, the solution was transferred to 100mL volumetric flask, constant volume, and mix.

4.7

tin standard solution, its configuration is as follows.

a) 1mg/mL tin standard stock solution. You can use a commercially available standard solution to meet the requirements or prepared as follows. Weigh 1.0000g

Tin (purity not less than 99.9%), placed in 200mL beaker, add 10mL water, 15mL of hydrochloric acid (4.1), taking close

Sealing measures to prevent solution evaporation, constant temperature (50 ± 2) °C heated to a metal tin is completely dissolved, cooling, the solution is transferred to 1000mL capacity

Flask with a volume fraction of 10% hydrochloric acid solution to volume, and mix.

GB/T 7094-2016 | CB 1146.8-1996 | CB 1146.9-1996 | GB/T 17848-2026 | GB/T 14616-2026 | GB/T 26084-2010 | […]

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This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 15 pages — is available in the English PDF.

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