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GB/T 25219-2010Inspection of grain and oils - Determination of starch content in maize - Near-infrared method (English PDF)

粮油检验 玉米淀粉含量测定 近红外法

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Issued by

SAMR; SAC

Level / Type

National · Recommended

Issue date

September 26, 2010

Implementation date

March 1, 2011

Scope

GB/T 25219-2010 is the English-translated version of 粮油检验 玉米淀粉含量测定 近红外法.

GB/T 25219-2010 is the Chinese standard "Inspection of grain and oils - Determination of starch content in maize - Near-infrared method".

Its scope clause reads: This standard specifies the method for the determination of NIR corn starch content (dry basis) of the terms and definitions, principles, equipment, measurement results Processing and presentation, and asked to confirm the process, and the accuracy and precision of the test report abnormal samples.

This standard applies to maize starch content (dry basis) of rapid determination. This standard does not apply to arbitration inspection. Its clauses include terms and definitions; equipment; determination.

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Document preview — GB/T 25219-2010

National Standard of the People's Republic of China

ICS
67.060
Classification
B 20

Issued by: State Administration for Market Regulation; Standardization Administration of the PRC

Contents

  • 1 Scope
  • 2 Normative references
  • 3 Terms and Definitions
  • 5 Equipment
  • 6 Determination

1 Scope

This standard specifies the method for the determination of NIR corn starch content (dry basis) of the terms and definitions, principles, equipment, measurement results

Processing and presentation, and asked to confirm the process, and the accuracy and precision of the test report abnormal samples.

This standard applies to maize starch content (dry basis) of rapid determination.

This standard does not apply to arbitration inspection.

2 Normative references

The following documents contain provisions which, through reference in this standard and become the standard terms. For dated references, subsequent

Amendments (not including errata content) or revisions do not apply to this standard, however, encourage the parties to the agreement are based on research

Whether the latest versions of these documents. For undated reference documents, the latest versions apply to this standard.

Determination of GB/T 5009.9 food starch

GB 5491 grain and oilseeds testing for sampling, and sample method

GB/T 24895 Inspection of grain NIR calibration model validation and network management and maintenance of general rules

3 Terms and Definitions

Terms and definitions GB/T 24895 regulations apply to this standard.

Principle 4

The use of starch molecules CH, NH, OH and other overtone vibration or rotation of the near-infrared light absorption characteristics of a chemical bond with technology

Chemometrics method to establish the correlation between corn near-infrared spectroscopy and its starch content between the calculated corn starch content of the sample.

5 Equipment

5.1 NIR analyzer

Add OILS NIR network equipment should comply with GB/T 24895 requirements. No added OILS near infrared

Analysis of network equipment, verify eligibility in accordance with GB/T 24895 in the provisions relating to the calibration model validation.

5.2

sample grinding equipment (for measuring powder samples NIR analyzer). particle size distribution and homogeneity of the crushed sample should be consistent with the past

Infrared analyzer calibration model established requirements when, should be used when using the same manufacturing process and model calibration and verification.

6 Determination

6.1 preparation before the test

6.1.1

Sampling and sample decimation executed according to the provisions of GB 5491.

6.1.2

Sample finishing, to remove impurities in the sample.

6.1.3

according to the near-infrared analyzer (5.1) specification requirements for instrument self-test and warm-up test.

6.1.4

In the case where the state of at least a day of near infrared analyzer (5.1) monitoring once with monitoring samples. It should track and monitor the results every day,

The measurement results of the same sample monitoring compared with the initial measurement result, shall ensure compliance with the provisions of 9.2. Monitor sample preparation in accordance with Appendix A

Regulations.

GB/T 15682-2008 | GB/T 22505-2008 | GB/T 22725-2008 | GB/T 25229-2024 | GB/T 25226-2010 | GB/T 25222-2010 | […]

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This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 15 pages — is available in the English PDF.

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