GB/T 18294.5-2010Technical identification methods for fire - Part 5: Gas chromatography-mass spectrometry analysis (English PDF)
火灾技术鉴定方法 第5部分:气相色谱-质谱法
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Issued by
SAMR; SAC
Level / Type
National · Recommended
Issue date
January 14, 2011
Implementation date
June 1, 2011
Scope
GB/T 18294.5-2010 is the English-translated version of 火灾技术鉴定方法 第5部分:气相色谱-质谱法.
GB/T 18294.5-2010 is the Chinese standard "Technical identification methods for fire - Part 5: Gas chromatography-mass spectrometry analysis". Its scope clause reads: This part of GB/T 18294 specifies the terms and definitions of gas chromatography-mass spectrometry (GC-MS) in fire technology identification.
Test equipment, test conditions and test methods. This part applies to gasoline, kerosene, diesel, paint thinner and other fire scene common flammable liquid and its combustion residue identification.
Its clauses include normative reference documents; terms and definitions; test principle; test equipment.
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Document preview — GB/T 18294.5-2010
National Standard of the People's Republic of China
- ICS
- 13.220.01
- Classification
- C 82
Issued by: State Administration for Market Regulation; Standardization Administration of the PRC
Contents
- 1 Scope
- 2 normative reference documents
- 3 terms and definitions
- 4 test principle
- 5 test equipment
1 Scope
This part of GB/T 18294 specifies the terms and definitions of gas chromatography-mass spectrometry (GC-MS) in fire technology identification.
Test equipment, test conditions and test methods.
This part applies to gasoline, kerosene, diesel, paint thinner and other fire scene common flammable liquid and its combustion residue identification.
2 normative reference documents
The following documents are indispensable for the application of this document. For dated references, only the dated edition applies to this article
Pieces. For undated references, the latest edition (including all modifications) applies to this document.
GB/T 19267.7 Physical and chemical testing of microchemical evidence for criminal technology - Part 7. Gas chromatography - mass spectrometry
GB/T .20162 Fire technology identification material extraction method
3 terms and definitions
GB/T 19267.7 and GB/T .20162 and the following terms and definitions apply to this document.
3.1 Total ion chromatogram
In the chromatographic conditions under which the flammable liquid is passed through a capillary column, the total ion current of each component obtained by mass spectrometry
The intensity varies with the scan time.
3.2 Extraction of ion - flow chromatograms
A map of the characteristic ion peaks of the flammable liquid selected from the total ion chromatogram.
4 test principle
After the laboratory pretreatment to be analyzed samples, injected into the gas chromatography-mass spectrometry instrument, after a pair of analytical samples with good
Good separation of the capillary column into the mass spectrum, the total ion chromatogram, using the total ion chromatogram and extraction of ion current chromatography
The characteristic of the flammable liquid is determined qualitatively by distinguishing the characteristic peaks.
5 test equipment
5.1 Gas Chromatography - Mass Spectrometer
A combination of a capillary chromatograph that separates flammable liquids and a mass spectrometer that identifies flammable liquids.
5.2 syringes
5.2.1 Liquid syringe
Volume injector in the range of 0.1 µL to 10.0 µL.
......
This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 15 pages — is available in the English PDF.
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Related Standards
GB/T 18294.6-2012 — Technical identification methods for fire - Part 6: Infrared spectroscopy analysis
GB/T 18294.4-2007 — Technical identification method for fire - Part 4: High performance liquid chromatography analysis
GB/T 18294.7-2026 — Technical identification methods for fire investigation - Part 7: X-ray imaging analysis
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