GB/T 14352.8-2010Methods for chemical analysis of tungsten ores and molybdenum ores - Part 8: Determination of nickel content (English PDF)
钨矿石、钼矿石化学分析方法 第8部分:镍量测定
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Issued by
General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China; Standardization Administration of China
Level / Type
National · Recommended
Issue date
November 10, 2010
Implementation date
February 1, 2011
Scope
GB/T 14352.8-2010 is the English-translated version of 钨矿石、钼矿石化学分析方法 第8部分:镍量测定.
GB/T 14352.8-2010 is Part 8 of the Chinese national series of methods for the chemical analysis of tungsten ores and molybdenum ores, and specifies the determination of nickel content.
It gives two methods: a polarographic method in a dimethylglyoxime - sulfosalicylic acid - ammonia - ammonium chloride supporting electrolyte, after sodium peroxide fusion and removal of iron with tributyl phosphate extraction resin, covering 5 µg/g to 500 µg/g of nickel; and a flame atomic absorption spectrophotometric method at 232.0 nm, after decomposition with hydrofluoric acid, aqua regia and perchloric acid, covering 10 µg/g to 1 000 µg/g.
For each method it sets out the reagents and standard solutions, apparatus, sample preparation and drying, test portion masses, blank and verification tests, calibration, calculation of results and precision data.
It replaces GB/T 14352.8-1993, which contained the polarographic method only: the atomic absorption method and safety warnings have been added and the sample drying temperature has been changed.
Issued on 10 November 2010, in force since 1 February 2011. Classification: ICS 73.060, CCS D40. The document runs to 12 pages, delivered complete in English translation.
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Document preview — GB/T 14352.8-2010
National Standard of the People's Republic of China
- ICS
- 73.060
- Classification
- D40
- Replacing
- GB/T 14352.8-1993
Issued by: General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China; Standardization Administration of China
Contents
- Foreword
- 1 Scope
- 2 Normative references
- 3 Polarography in a dimethylglyoxime-sulfosalicylic acid-ammonia-ammonium chloride base solution
- 4 Flame atomic absorption spectrophotometry
3 Polarography in a dimethylglyoxime-sulfosalicylic acid-ammonia-ammonium chloride base solution
4 Flame atomic absorption spectrophotometry
Foreword
GB/T 14352, Methods for chemical analysis of tungsten ores and molybdenum ores, consists of 18 parts:
- Part 1: Determination of tungsten content;
- Part 2: Determination of molybdenum content;
- Part 3: Determination of copper content;
- Part 4: Determination of lead content;
- Part 5: Determination of zinc content;
- Part 6: Determination of cadmium content;
- Part 7: Determination of cobalt content;
- Part 8: Determination of nickel content;
- Part 9: Determination of sulfur content;
- Part 10: Determination of arsenic content;
- Part 11: Determination of bismuth content;
- Part 12: Determination of silver content;
- Part 13: Determination of tin content;
- Part 14: Determination of gallium content;
- Part 15: Determination of germanium content;
- Part 16: Determination of selenium content;
- Part 17: Determination of tellurium content;
- Part 18: Determination of rhenium content.
This part is Part 8 of GB/T 14352.
This part replaces GB/T 14352.8-1993, Methods for chemical analysis of tungsten ores and molybdenum ores - Determination of nickel content by polarography in dimethylglyoxime - sulfosalicylic acid - ammonium hydroxide - ammonium chloride supporting electrolyte.
Compared with GB/T 14352.8-1993, the main changes in this part are as follows:
- a flame atomic absorption spectrometric method for the determination of nickel content has been added;
- warning and caution statements have been added;
- the drying temperature of the sample has been modified.
Annex A of this part is informative.
This part was proposed by the Ministry of Land and Resources of the People's Republic of China.
This part is under the jurisdiction of the National Technical Committee for Standardization of Land and Resources.
Responsible drafting organization of this part: National Research Center for Geoanalysis.
Drafting organization of this part: Geological Survey of Jiangsu Province (Nanjing Mineral Resources Supervision and Testing Center, Ministry of Land and Resources).
Chief drafters of this part: Huang Guangming, Tang Zhiyun, Jiang Ye.
The previous editions of the standard replaced by this part are:
- GB/T 14352.8-1993.
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This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 12 pages — is available in the English PDF.
Referenced standards
Similar standards
Editions of GB/T 14352.8
| Edition | Title | Revision | Status |
|---|---|---|---|
| GB/T 14352.8-2010 | Methods for chemical analysis of tungsten ores and molybdenum ores - Part 8: Determination of nickel content | current edition | Current |
| GB/T 14352.8-1993 | Methods for chemical analysis of tungsten ores and molybdenum ores. Determination of nickel content. Polarographic method in dimethylg-lyoxime-sulfosalicylic acid-ammonium hydroxide-ammonium chloride system | previous edition | Superseded |
This page sells the current edition, GB/T 14352.8-2010. Earlier editions are listed for reference only.
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GB/T 14352.1-2010 — Methods for chemical analysis of tungsten ores and molybdenum ores - Part 1: Determination of tungsten content
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