GB/T 12690.5-2017Chemical analysis methods for non-rare earth impurities in rare earth metals and their oxides - Part 5: Determination of cobalt, manganese, lead, nickel, copper, zinc, aluminium, chromium, magnesium, cadmium, vanadium and iron (English PDF)
稀土金属及其氧化物中非稀土杂质化学分析方法 第5部分:钴、锰、铅、镍、铜、锌、铝、铬、镁、镉、钒、铁量的测定
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Issued by
General Administration of Quality Supervision, Inspection and Quarantine; Standardization Administration of the PRC
Level / Type
National · Recommended
Issue date
October 14, 2017
Implementation date
February 1, 2018
Scope
GB/T 12690.5-2017 is the English-translated version of 稀土金属及其氧化物中非稀土杂质化学分析方法 第5部分:钴、锰、铅、镍、铜、锌、铝、铬、镁、镉、钒、铁量的测定.
GB/T 12690.5-2017 is the Chinese standard "Chemical analysis methods for non-rare earth impurities in rare earth metals and their oxides - Part 5: Determination of cobalt, manganese, lead, nickel, copper, zinc, aluminium, chromium, magnesium, cadmium, vanadium and iron".
Its scope clause reads: GB/T 12690 provisions of this part of cobalt, manganese, lead, nickel, copper, zinc, aluminum, chromium, magnesium, cadmium, vanadium, iron content of rare earth metals and their oxidation Oxides of cobalt, manganese oxide, lead oxide, nickel oxide, copper oxide, zinc oxide, aluminum oxide, chromium oxide, magnesium oxide, cadmium oxide, vanadium oxide, iron oxide Determination of content.
This section applies to cobalt, manganese, lead, nickel, copper, zinc, aluminum, chromium, magnesium, cadmium, vanadium, iron content and oxides of rare earth metals cobalt oxide, oxidation Determination of manganese, lead oxide, nickel oxide, copper oxide, zinc oxide, aluminum oxide, chromium oxide, magnesium oxide, cadmium oxide, vanadium oxide, iron oxide content.
Total package Two methods are included. Method 1 Inductively coupled plasma atomic emission spectrometry, Method 2 Inductively coupled plasma mass spectrometry.
Method 1 Measurement range See Table 1, Method 2 determination range in Table 2.
Table 1 Oxide measurement range (mass fraction) /% Oxide measurement range (mass fraction) /% Cobalt oxide 0.0010 to 0.10 Alumina 0.0010 to 0.10 Manganese oxide 0.0010 to 0.10 Chromium oxide 0.0010 to 0.10 Lead oxide 0.0010 to 0.10 Magnesium oxide 0.0002 to 0.10 Nickel oxide 0.0010 to 0.10 Cadmium oxide 0.0010 to 0.10 Copper oxide 0.0010 to 0.10 Vanadium oxide 0.0010 to 0.10 Zinc oxide 0.0010 to 0.10 Iron oxide 0.0010 to 0.50 Table 2 Oxide measurement range (mass fraction) /% Oxide measurement range (mass fraction) /% Cobalt oxide 0.0001 to 0.050 Alumina 0.0003 to 0.050 Manganese oxide 0.0001 to 0.050 Chromium oxide 0.0001 to 0.050 Lead oxide 0.0001-0.050 Magnesia 0.0001-0.050 Nickel oxide 0.0001 to 0.050 Cadmium oxide 0.0001 to 0.050 Copper oxide 0.0001 to 0.050 Vanadium oxide 0.0001 to 0.050 Zinc oxide 0.0003 to 0.050 - -. Its clauses include methods 1.
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Document preview — GB/T 12690.5-2017
National Standard of the People's Republic of China
- ICS
- 77.120.99
- Classification
- H 14
- Replacing
- GB/T 12690.5-2003
Issued by: General Administration of Quality Supervision, Inspection and Quarantine; Standardization Administration of the PRC
Contents
- 0.10 Alumina 0.0010 to
- 0.50 Table
- 1 Scope
- 2 Methods 1. Inductively coupled plasma atomic emission spectrometry
1 Scope
GB/T 12690 provisions of this part of cobalt, manganese, lead, nickel, copper, zinc, aluminum, chromium, magnesium, cadmium, vanadium, iron content of rare earth metals and their oxidation
Oxides of cobalt, manganese oxide, lead oxide, nickel oxide, copper oxide, zinc oxide, aluminum oxide, chromium oxide, magnesium oxide, cadmium oxide, vanadium oxide, iron oxide
Determination of content.
This section applies to cobalt, manganese, lead, nickel, copper, zinc, aluminum, chromium, magnesium, cadmium, vanadium, iron content and oxides of rare earth metals cobalt oxide, oxidation
Determination of manganese, lead oxide, nickel oxide, copper oxide, zinc oxide, aluminum oxide, chromium oxide, magnesium oxide, cadmium oxide, vanadium oxide, iron oxide content. Total package
Two methods are included. Method 1 Inductively coupled plasma atomic emission spectrometry, Method 2 Inductively coupled plasma mass spectrometry. Method 1 Measurement range
See Table 1, Method 2 determination range in Table 2.
Table 1
Oxide measurement range (mass fraction) /% Oxide measurement range (mass fraction) /%
Cobalt oxide 0.0010 to 0.10 Alumina 0.0010 to 0.10
Manganese oxide 0.0010 to 0.10 Chromium oxide 0.0010 to 0.10
Lead oxide 0.0010 to 0.10 Magnesium oxide 0.0002 to 0.10
Nickel oxide 0.0010 to 0.10 Cadmium oxide 0.0010 to 0.10
Copper oxide 0.0010 to 0.10 Vanadium oxide 0.0010 to 0.10
Zinc oxide 0.0010 to 0.10 Iron oxide 0.0010 to 0.50
Table 2
Oxide measurement range (mass fraction) /% Oxide measurement range (mass fraction) /%
Cobalt oxide 0.0001 to 0.050 Alumina 0.0003 to 0.050
Manganese oxide 0.0001 to 0.050 Chromium oxide 0.0001 to 0.050
Lead oxide 0.0001-0.050 Magnesia 0.0001-0.050
Nickel oxide 0.0001 to 0.050 Cadmium oxide 0.0001 to 0.050
Copper oxide 0.0001 to 0.050 Vanadium oxide 0.0001 to 0.050
Zinc oxide 0.0003 to 0.050 - -
2 Methods 1
Inductively coupled plasma atomic emission spectrometry
2.1 method principle
The sample was dissolved in nitric acid, excited in a dilute nitric acid medium by an argon plasma light source, and subjected to spectrometry. […]
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This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 30 pages — is available in the English PDF.
Referenced standards
Normative references
- GB/T 6682Water for analytical laboratory use - Specification and test methods
- GB/T 8170Rules of rounding off for numerical values & expression and judgement of limiting values
- GB/T 12690.1Chemical analysis methods for non-rare earth impurities of rare earth metals and their oxides - Part 1: Determination of carbon and sulfur contents - High frequency-infrared absorption method
- GB/T 17803Designation system for rare earth products
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Related Standards
GB/T 12690.1-2022 — Chemical analysis methods for non-rare earth impurities of rare earth metals and their oxides - Part 1: Determination of carbon and sulfur contents - High frequency-infrared absorption method
GB/T 12690.10-2003 — Chemical analysis methods for non-rare earth impurities of rare earth metals and their oxides--Determination of phosphorus content by molybdenum blue spectrophotometric method
GB/T 12690.11-2025 — Chemical analysis methods for non-rare earth impurities of rare earth metals and their oxides - Part 11: Determination of magnesium content - Flame atomic absorption spectrometric method
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