Valid

GB 2463-1981Pyrites and concentrate -- Determination of total iron content -- Cerium sulfate volumetric and potassium dichromate volumetric methods (English PDF)

Preview PDF

Also coversGB2463-1981

This is a limited preview

Buy now to download the full PDF (6 pages)

Need quotation for your management?

Get a formal quotation for GB 2463-1981 in 30 minutes.

Issued by

Standardization Administration of China

Level / Type

National · Mandatory

Issue date

May 14, 2008

Implementation date

October 1, 2008

Scope

GB 2463-1981 (Pyrites and concentrate -- Determination of total iron content -- Cerium sulfate volumetric and potassium dichromate volumetric methods) is available as an English-translated PDF.

GB 2463-1981 — This standard specifies the Pyrites and concentrate - total iron content of sulfuric acid and potassium dichromate volumetric method cerium volumetric method.

This standard applies to Pyrites and concentrate products total iron content greater than 10% was measured.

Found what you need?

Document preview — GB 2463-1981

National Standard of the People's Republic of China

ICS
73.060.01
Classification
D 51
Replacing
GB/T 2463.1-1996; GB/T 2463.2-1996

Issued by: Standardization Administration of China

Contents

  • Foreword
  • 1 Scope
  • 2 Normative references
  • 3 Sample
  • 4 General Provisions
  • 5 Analysis
  • 5.1 Cerium sulfate volumetric method

Foreword

This standard replaces GB/T 2463.1-1996 "Pyrites and concentrate - Determination of total iron content - Part 1. Cerium sulfate volumetric method" and GB/T 2463.2-1996 "Pyrites and concentrate - Determination of total iron content - Part 2. Titanium trichloride - potassium dichromate volumetric method" these two criteria are combined into a standard, divided into two methods.

The standard proposed by China Petroleum and Chemical Industry Association.

This standard is under the jurisdiction of Chemical Industry Standardization Technical Committee chemical mine.

This standard was drafted. even in the blue sea and Design Institute.

1 Scope

This standard specifies the Pyrites and concentrate - total iron content of sulfuric acid and potassium dichromate volumetric method cerium volumetric method.

This standard applies to Pyrites and concentrate products total iron content greater than 10% was measured.

2 Normative references

The following documents contain provisions which, through reference in this standard and become the standard terms. For dated references, subsequent Amendments (not including errata content) or revisions do not apply to this standard, however, encourage the parties to the agreement are based on research Whether the latest versions of these documents. For undated reference documents, the latest versions apply to this standard.

GB/T 6003.1 woven wire mesh test sieve (GB/T 6003.1-1997, eqv ISO 3310-1:1990) GB/T 6682 analytical laboratory use specifications and test methods (GB/T 6682-1992, neq ISO 3696. 1987)

3 Sample

The sample passes through 150µm test sieve (GB/T 6003.1), at 100 °C ~ 105 °C drying to constant weight, placed in a desiccator, cooled to Room temperature.

4 General Provisions

The water of this standard shall comply with GB/T 6682 water in three specifications; reagents listed Unless otherwise specified, refer to analytical reagent.

5 Analysis

5.1 Cerium sulfate volumetric method

5.1.1 Method summary

Samples with sodium hydroxide, sodium peroxide melt in hydrochloric acid medium, with hypophosphite reducing ferric ions, sodium for diphenylamine Indicator, cerium sulfate standard titration solution titration, you can find the total iron content.

5.1.2 Reagents and solutions

5.1.2.1 sodium hydroxide.

5.1.2.2 sodium peroxide.

5.1.2.3 hydrochloric acid solution. 1 + 1.

5.1.2.4 hypophosphite solution. 100g/L.

5.1.2.5 sodium sulfite anhydrous. 1g/L.

5.1.2.6 sulfuric acid - phosphoric acid mixed solution. stirring the sulfuric acid was slowly added to 500mL 200mL water, then adding cooled 300mL phosphoric acid, and mix.

5.1.2.7 ferrous ammonium sulfate solution. 0.05mol/L. Weigh 1.96g of ferrous ammonium sulfate [(NH4) 2Fe (SO4) 2 · 6H2O] was dissolved in a small the amount of water, add 10 drops of sulfuric acid and transferred to 100mL volumetric flask, dilute to the mark, shake.

5.1.2.8 Iron standard solution. 1.00mg/L. Weigh 1.4297g ferric oxide (high purity) in 250mL beaker, add 50mL Hydrochloric acid solution, cover the surface of the pan, over low heat to dissolve completely cooled and transferred to 1000mL volumetric flask, dilute to the mark, shake. this Solution of iron (Fe) the amount of 1.00mg/mL.

......
This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 6 pages — is available in the English PDF.

Referenced standards

How to Download GB 2463-1981

  1. 1

    Add to cart

    Click "Download PDF" on this page and choose "Buy this standard". You can add more standards before checkout.

  2. 2

    Checkout

    Enter your email and billing details. Payment is processed securely by Stripe (cards or bank transfer). Prefer bank details? Request a quotation (min. order $300).

  3. 3

    Instant delivery (0–9 sec)

    Delivery is automatic: within seconds of payment you'll receive an email with a secure download link. The link stays valid for 72 hours.

  4. 4

    Invoice included

    A tax invoice is attached to the confirmation email. Need a custom invoice? Contact us.

Related Standards

English PDF
6 pages
Instant delivery (0–9 sec)
Invoice included
View Cart

Secure payment via Stripe

Payments accepted

VisaMastercardAmerican ExpressApple PayGoogle PayStripe

GB 2463-1981

$155.00