YS/T 461.12-2016Methods for chemical analysis of lead and zinc bulk concentrates--Part 12: Determination of thallium content--Inductively coupled plasma mass spectrometry and inductively coupled plasma atomic emission spectrometry (English PDF)

Foreword

YS/T 461 "mixed lead and zinc concentrate chemical analysis method" is divided into 12 parts.

- Part 1. Determination of lead content and zinc content - Separation of Na2EDTA titration;

- Part 2. Determination of iron content - Na2EDTA titration;

- Part 3. Determination of sulfur content - Combustion - neutralization titration;

- Part 4. Determination of arsenic iodine titration;

- Part 5. Determination of the amount of silica - Molybdenum blue spectrophotometric method;

- Part 6. Determination of mercury content - Atomic fluorescence spectrometry;

- Part 7. Determination of cadmium content - Flame atomic absorption spectrometric method;

- Part 8. Determination of copper content - Flame atomic absorption spectrometric method;

- Part 9. Determination of silver content - Flame atomic absorption spectrometric method;

- Part 10. Determination of gold and silver;

- Part 11. Determination of arsenic, bismuth, cadmium, cobalt, copper, nickel and antimony - Inductively coupled plasma - atomic emission spectrometry;

Part 12. Determination of thallium content - Inductively coupled plasma mass spectrometry and inductively coupled plasma atomic emission spectrometry.

This part is part 12 of YS/T 461.

This part is drafted in accordance with the rules given in GB/T 1.1-2009.

This part of the National Nonferrous Metals Standardization Technical Committee (SAC/TC243) proposed and centralized.

The main method of this part of the main drafting unit. Shenzhen Jinling South Nonferrous Metals Co., Ltd. Shaoguan smelter, Shaoguan quality measurement Supervisor.

Part 2 Method 2 Main Drafting Unit. Fangchenggang Entry-Exit Inspection and Quarantine Bureau.

This part participates in the drafting unit. Beijing Mining and Metallurgy Research Institute, China Nonferrous Guilin Mineral Geology Research Institute Co., Ltd., Zijin Mining Group Co., Ltd., Ningbo Entry-Exit Inspection and Quarantine Bureau Technology Center, Kunming Metallurgical Research Institute.

The main method of this part of the main drafters. Yuan Qi, Zhang Xiaojun, Shi Shilong, Zhu Ling, Liu Runting, Su Chunfeng, the ancient line, Tang Biyu, Luo Wen, Xie Wenliang, Shi Honglan, Zhu Xiaoyan, Li Chao, Liu Weili.

This part of the method 2 main drafters. Luo Minggui, Li Xiangrong, Chen Zhipeng, Su Chunfeng, Qiu Li, Wang Jiangliang, Luo Wen, Yu Jinsheng, Yang Jianbing, Huang Zufei, Shi Honglan, Cao Guozhou.

Chemical Analysis of Mixed Lead - Zinc Concentrate Part 12. determination of thallium content Inductively coupled plasma mass spectrometry and inductively coupled plasma atomic emission spectrometry

1 Scope

This part of YS/T 461 specifies the method for the determination of thallium in mixed lead-zinc concentrates.

This part is applicable to the determination of thallium in mixed lead and zinc concentrates. Method 1 has a measurement range of 0.000050% to 0.010%; Method 2 is measured the range is 0.0050% ~ 0.10%. Section 1 Scope Cross Section Method 1 is an arbitration method.

2 Method 1 Inductively Coupled Plasma Mass Spectrometry