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SN/T 2765.2-2013Determination of arsenic, chromium, cadimium, lead and mercury in iron ores. Inductively coupled plasma mass spectrometry(ICP-MS) (English PDF)

铁矿石中砷、铬、镉、铅、汞的测定 电感耦合等离子体-质谱法

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Issued by

General Administration of Customs

Level / Type

National · Recommended

Issue date

March 1, 2013

Implementation date

September 16, 2013

Scope

SN/T 2765.2-2013 is the English-translated version of 铁矿石中砷、铬、镉、铅、汞的测定 电感耦合等离子体-质谱法.

SN/T 2765.2-2013 - This section SN/T 2765 specifies the inductively coupled plasma iron ore of arsenic, chromium, cadmium, lead and mercury - mass spectrometry.

This section applies to arsenic, chromium, cadmium, lead and mercury in iron ore measured, the measurement range of each element in Table 1. Table 1 measurement range of each element Element Measuring range/(µg/kg) element Measuring range/(µg/kg) Arsenic 2.53 0.40 3200 to 1900 lead Chromium 1.83 6.27 ~ 190 ~ 2500 Mercury Cadmium 0.15 ~ 0.55

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Document preview — SN/T 2765.2-2013

National Standard of the People's Republic of China

ICS
73.060.10
Classification
D31

Issued by: General Administration of Customs

Contents

  • Foreword
  • 1 Scope
  • 2 Normative references
  • 3 Method summary
  • 4 Reagents and materials
  • 4.1 Pairs of reagents and materials requirements
  • 4.2 Preparation of the solution

Foreword

This section SN/T Section 22765 of.

This section drafted in accordance with GB/T 1.1-2009 given rules.

This section proposed and managed by the National Certification and Accreditation Administration Committee.

1 Scope

This section SN/T 2765 specifies the inductively coupled plasma iron ore of arsenic, chromium, cadmium, lead and mercury - mass spectrometry.

This section applies to arsenic, chromium, cadmium, lead and mercury in iron ore measured, the measurement range of each element in Table 1.

Table 1 measurement range of each element

Element Measuring range/(µg/kg) element Measuring range/(µg/kg) Arsenic 2.53 0.40 3200 to 1900 lead Chromium 1.83 6.27 ~ 190 ~ 2500 Mercury Cadmium 0.15 ~ 0.55

2 Normative references

The following documents for the application of this document is essential. For dated references, only the dated version suitable for use herein Member. For undated references, the latest edition (including any amendments) applies to this document.

Laboratory use specifications and test methods GB/T 6682-2008 Analysis GB/T 10322.1 iron ore sampling and sample preparation methods

3 Method summary

Samples using high temperature pressure microwave digestion process was diluted to volume with water, using the internal standard line, directly inductively coupled plasma Body - mass spectrometry (ICP-MS) was measured.

4 Reagents and materials

4.1 Pairs of reagents and materials requirements

Reagents used in this standard is pure class system or steamed acid-treated chemical reagents, test water should be consistent with GB/T 6682-2008 A water specified.

4.1.1 hydrochloric acid (rho = 1.19g/mL).

4.1.2 hydrofluoric acid (rho = 1.13g/mL).

4.1.3 nitric acid (rho = 1.4g/mL).

4.1.4 purity argon gas (purity greater than 99.999%).

4.2 Preparation of the solution

4.2.1 2% nitric acid (298) solution. take the right amount of nitric acid (4.1.3) and ultra-pure water volume ratio of 2.98 were mixed.

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This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 6 pages — is available in the English PDF.

Referenced standards

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