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GB/T 38257-2019Laser-induced breakdown spectroscopy (English PDF)

激光诱导击穿光谱法

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Issued by

SAMR; SAC

Level / Type

National · Recommended

Issue date

December 10, 2019

Implementation date

July 1, 2020

Scope

GB/T 38257-2019 is the English-translated version of 激光诱导击穿光谱法.

GB/T 38257-2019 is the Chinese standard "Laser-induced breakdown spectroscopy". Its scope clause reads: This standard specifies the terms and definitions, basic principles, test conditions, equipment and devices, samples, and test procedures of laser-induced breakdown spectroscopy.

Procedures, data processing and test reports. This standard applies to the detection and analysis of chemical elements of solid, liquid and gaseous substances. Its clauses include terms and definitions.

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Document preview — GB/T 38257-2019

National Standard of the People's Republic of China

ICS
17.180.99
Classification
L 50

Issued by: State Administration for Market Regulation; Standardization Administration of the PRC

Contents

  • Foreword
  • 1 Scope
  • 2 Normative references
  • 3 Terms and definitions
  • 4 Basic principles
  • 5 Test conditions
  • 6 Equipment and devices
  • 6.1 Component
  • 6.2 Laser light source system
  • 6.3 Laser focusing system
  • 6.4 Plasma radiation collection system
  • 6.5 Spectrometer
  • 6.6 Control circuit and data processing system
  • 7 Sample
  • 7.1 Samples and substances to be analyzed
  • 7.2 Matrix effects of the sample
  • 7.3 Non-uniformity of the sample
  • 7.4 Sample preparation and pretreatment
  • 8 Test step
  • 8.1 Start-up warm-up
  • 8.2 Parameter setting
  • 8.3 Calibration of Spectrum Intensity
  • 8.4 Spectral Acquisition
  • 8.5 Spectral preprocessing
  • 9 Data processing
  • 9.1 Qualitative analysis
  • 9.2 Quantitative analysis
  • 9.3 Semi-Quantitative Analysis
  • 10 Test report
  • Appendix A (informative) Test report format

1 Scope

This standard specifies the terms and definitions, basic principles, test conditions, equipment and devices, samples, and test procedures of laser-induced breakdown spectroscopy.

Procedures, data processing and test reports.

This standard applies to the detection and analysis of chemical elements of solid, liquid and gaseous substances.

2 Normative references

The following documents are essential for the application of this document. For dated references, only the dated version applies to this article

Pieces. For undated references, the latest version (including all amendments) applies to this document.

GB 7247.1 Safety of laser products. Part 1. Equipment classification and requirements

GB/T 13966-2013 terminology for analytical instruments

GB/T 14666-2003 Analytical Chemistry Terms

3 terms and definitions

The terms and definitions defined in GB/T 13966-2013 and GB/T 14666-2003 and the following apply to this document.

3.1

Plasma is formed by laser ablation of the substance to be analyzed, in which excited atoms, ions or molecules transition to low energy levels or ground states

At that time, photons with a specific energy are emitted outward to form a characteristic spectrum, thereby obtaining the chemical composition or other characteristics of the substance to be analyzed.

3.2 Laser-induced plasma

Plasma generated by laser ablation.

Note. The above plasma generally contains electrons, atoms, molecules, positive and negative ions, and micro-nano particles.

3.3 Standard sample

It has the accuracy to meet the needs of analysis, assign value to the substance to be analyzed, evaluate the measurement method, and calibrate or verify the substance of the equipment.

3.4 Calibration curve

Under specified conditions, it represents the relationship between the content of the element to be analyzed and the measured spectral intensity value.

Note 1. The calibration curve is also called the calibration curve.

Note 2. Rewrite GB/T 13966-2013, definition 2.89.

3.5 Qualitative analysis

Determine whether the element to be analyzed contains the element according to the characteristic spectral line of the laser-induced plasma spectrum

Analytical methods.

Note 1. Analytical methods for classifying substances based on spectral characteristics are also called qualitative analysis.

Note 2. Rewrite GB/T 13966-2013, definition 2.2.

GB/T 7962.13 | GB/T 7962.7 | GB/T 41310 | GB/T 18310.10 | GB/T 38256 | […]

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This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 14 pages — is available in the English PDF.

Referenced standards

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