GB/T 33912-2017Wrought aluminum and aluminum alloy ingots made of high pure materials (English PDF)
高纯金属为原料的变形铝及铝合金铸锭
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Issued by
SAMR; SAC
Level / Type
National · Recommended
Issue date
July 12, 2017
Implementation date
June 1, 2018
Scope
GB/T 33912-2017 is the English-translated version of 高纯金属为原料的变形铝及铝合金铸锭.
GB/T 33912-2017 is the Chinese national standard for wrought aluminium and aluminium alloy ingots made of high pure materials, and this record is served with the official English translation.
It specifies the requirements, the test methods, the inspection rules, the marks, the packaging, the transport and the storage, together with the contents of the quality certificate and of the order sheet or contract.
The requirements fix the purity level of the main raw material, the chemical composition of the designations Al99.99, Al99.998, Al99.999 and Al99.9995 and of the designations 1G50, 4G60, 5G82 and 6G61, the hydrogen and slag content, the dimensions of round and flat ingots, the macrostructure, the grain size and the appearance quality, and they give the marking sequence of product name, standard reference, purity level, designation and dimensions with worked examples.
The test methods cover chemical analysis with the rounding-off comparison method, liquid-state and solid-state hydrogen measurement, size deviation, macrostructure, microstructure and appearance.
It applies to wrought aluminium and aluminium alloy ingots that require a low content of impurity elements. It cites GB/T 3190, GB/T 3199, GB/T 3246.1, GB/T 3246.2, GB/T 7999, GB/T 8170, GB/T 17432 and GB/T 20975. It was issued on 12 July 2017 and has applied since 1 June 2018.
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Document preview — GB/T 33912-2017
National Standard of the People's Republic of China
- ICS
- 77.150.10
- Classification
- H 61
Issued by: State Administration for Market Regulation; Standardization Administration of the PRC
Contents
- Foreword3
- 1 Scope4
- 2 Normative references4
- 3 Requirements5
- 4 Test methods10
- 5 Inspection rules12
- 6 Marks, packaging, transport, storage and quality certificate14
- 7 Contents of order sheet (or contract)15
1 Scope
This Standard specifies requirements, test methods, inspection rules, marks, packaging, transport, storage as well as contents quality certificate and order sheet (or content) for wrought aluminum and aluminum alloy ingots made of high pure materials.
This Standard is applicable to wrought aluminum and aluminum alloy ingots that require low content of impurity elements (hereinafter referred to as ingots).
2 Normative references
The following referenced documents are indispensable for the application of this document. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies.
GB/T 3190, Wrought aluminum and aluminum alloys - Chemical composition limits
GB/T 3199, Wrought aluminum and aluminum alloy products-Packing, marking, transporting and storing
GB/T 3246.1, Inspection method for structure of wrought aluminum and aluminum alloy products - Part 1: Inspection method for microstructure
GB/T 3246.2, Inspection method for structure of wrought aluminum and aluminum alloy products - Part 2: Inspection method for macrostructure
GB/T 7999, Optical emission spectrometric analysis method of aluminum and aluminum alloys
GB/T 8170, Rules of rounding off for numerical values & expression and judgement of limiting values
GB/T 17432, Methods for sampling for analyzing the chemical composition of wrought aluminum and aluminum alloys
GB/T 20975 (all parts), Methods for chemical analysis of aluminum and aluminum alloys
3 Requirements
extremely low content of impurity element.
3.1.2 Dimensions
Dimensions of round ingots shall comply with provisions of YS/T 67.
Dimensions of flat ingots shall comply with provisions of YS/T 590.
3.1.3 Marks and examples
Ingot marks shall be represented according to a sequence of product name, reference to standard, purity level of main raw material, designation, dimensions. Marking examples are as follows: Example 1:
Flat ingots of which designation is Al99.99, purity level of main raw material is 4N, thickness is 420mm, width is 1620mm, length is 6000mm, are marked as follow: Flat ingots GB/T 33912-4NAl99.99 420×1620×6000 Example 2:
Round ingots of which designation is 1G50, purity level of main raw material is 5N, diameter is 220mm, length is 6000mm, are marked as follow: Round ingots GB/T 33912-5N1G50 Phi220×6000
3.2 Chemical composition
3.2.1 Chemical composition of main raw material shall comply with provisions of Table 2. Chemical composition of other raw material shall be indicated in order sheet (or contract) after supplier and purchaser negotiate. When it is not indicated, it shall be decided by supplier.
3.2.2 Chemical composition of ingots of which designations are Al99.99, Al99.998, Al99.999, Al99.9995 shall comply with provisions of Table 2.
Chemical composition of ingots of which designations are 1G50, 4G60, 5G82, 6G61 shall comply with provisions of Table 3.
4 Test methods
Arbitration analysis shall adopt method specified in GB/T 20975 or method agreed by supplier and purchaser.
4.1.2 Conventional chemical analysis is only carried out for elements that have numerical regulation other than columns of "Al" and "Other" in Table 2, Table 3.
When it is suspected that mass fraction of non-conventional analysis elements exceeds limit value of this Standard, manufacturer shall analyze these elements.
4.1.3 "Al" content is calculated by method specified in GB/T 3190. When calculating "Al" content, take the sum of analysis values of conventional analysis element and suspected excess unconventional analysis elements as "Sum of element content".
4.1.4 Determination of analysis value uses rounding-off comparison method.
Value rounding-off rules are in accordance with relevant provisions in GB/T 8170. Rounding-off digit shall be the same as limit digit specified in Table 2, Table 3 or agreed between supplier and purchaser.
4.2 Hydrogen content
4.2.1 Testing of hydrogen content may use online liquid-state hydrogen measurement or solid-state hydrogen measurement. In arbitration, it shall use solid-state hydrogen measurement.
4.2.2 Liquid-state hydrogen measurement method shall be in accordance with provisions on closed-loop method in YS/T 600-2009.
4.2.3 Solid-state hydrogen measurement method shall be in accordance with provisions in Annex B of GB/T 33911-2017.
4.3 Slag content
Inspection method for slag content shall be determined by supplier and purchaser after negotiation.
4.4 Size deviation
Testing method for size deviation of round ingots shall be in accordance with method specified in YS/T 67. Testing method for size deviation of flat ingots shall be in accordance with method specified in YS/T 590.
4.5 Macrostructure
Inspection method for macrostructure shall be in accordance with provisions of GB/T 3246.2.
4.6 Microstructure
Inspection of grain size shall be performed according to provisions of GB/T 3246.1.
4.7 Appearance quality
Under natural scattered light, visually check appearance quality. When necessary, it may borrow dimensional measurement tools to define defect size. Determine defect depth by grinding.
5 Inspection rules
5.6.6 When appearance quality of any ingot fails, this ingot shall be rejected.
5.1 Inspection and acceptance
5.1.1 Ingots are inspected by supplier to ensure ingot quality complies with provisions of this Standard and order sheet (or contract). Fill quality certificate by supplier.
5.1.2 Purchaser shall inspect received ingots according to this Standard. When inspection results fail to comply with provisions of this Standard and order sheet (or contract), it shall be proposed to supplier in written form and be solved by supplier and purchaser after negotiation. Objections to appearance quality and size deviation shall be proposed within one month since ingots are received.
Objections to other performances shall be proposed within three months since ingots are received. If arbitration is required, it may entrust authority recognized by supplier and purchaser to perform. Sampling shall be conducted jointly at purchaser's site.
5.2 Batching
Ingots shall be submitted for acceptance in batches. Each batch shall be composed of ingots of same furnace time (or two furnace times), of same dimensions.
5.3 Weighing
Ingots shall be weighed out.
5.4 Inspection items
5.4.1 Each batch of ingots shall be subject to inspections of chemical composition, size deviation and appearance quality.
5.4.2 Selectively check hydrogen content, slag content, grain size and macrostructure.
5.5 Sampling
Only accepted products are delivered.
6 Marks, packaging, transport, storage and quality certificate
6.1 Marks
On side and sawing upper part of ingots that are inspected as accepted, print mark that contains following information (or stick label that contains following information):
a) inspection seal of supplier's quality inspection department (signature or stamp of inspector);
b) melting sequence number, designation and dimensions;
c) product lot number or date of production.
6.2 Packaging
Ingots are not applied with oils, are not packed in case. Others are in accordance with GB/T 3199. If oil application, casing or packing mode, method different from GB/T 3199 is required, it shall be agreed by supplier and purchaser and indicated in order sheet (or contract).
6.3 Transport and storage
Transport and storage of ingots shall comply with provisions of GB/T 3199.
6.4 Quality certificate
Each batch of ingots shall be attached with quality certificate, indicating:
a) supplier's name;
b) product name and dimensions;
c) designation;
d) melting sequence number;
e) weight, number of pieces;
f) reference to this Standard; […]
......
This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 15 pages — is available in the English PDF.
Referenced standards
Normative references
- GB/T 3190Chemical composition of wrought aluminium and aluminium alloys
- GB/T 3199Packing, marking, transport and storage of wrought aluminium and aluminium alloy products
- GB/T 3246.1Inspection method for structure of wrought aluminium and aluminium alloy products—Part 1: Inspection method for microstructure
- GB/T 3246.2Inspection methods for the structure of wrought aluminium and aluminium alloy products - Part 2: Inspection method for macrostructure
- GB/T 7999Photoelectric direct reading atomic emission spectrometric analysis of aluminium and aluminium alloys
- GB/T 8170Rules of rounding off for numerical values & expression and judgement of limiting values
GB/T 20975
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Related Standards
GB/T 17432-2012 — Methods of sampling for analyzing the chemical composition of wrought aluminum and aluminum alloys
GB/T 20975.1-2018 — Methods for chemical analysis of aluminium and aluminium alloys—Part 1: Determination of mercury content
GB/T 20975.10-2020 — Methods for chemical analysis of aluminium and aluminium alloys—Part 10: Determination of tin content
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