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GB/T 29024.4-2017Determination of particle size distribution -- Single particle light interaction methods -- Part 4: Light scattering airborne particle counter for clean spaces (English PDF)

粒度分析 单颗粒的光学测量方法 第4部分:洁净间光散射尘埃粒子计数器

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Issued by

General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China

Level / Type

National · Recommended

Issue date

September 29, 2017

Implementation date

April 1, 2018

Scope

GB/T 29024.4-2017 is the English-translated version of 粒度分析 单颗粒的光学测量方法 第4部分:洁净间光散射尘埃粒子计数器.

GB/T 29024.4-2017 specifies how a light scattering airborne particle counter (LSAPC) for clean spaces is calibrated and verified. The counter sizes airborne particles and counts their number concentration by light scattering from single particles, typically from 0.1 µm to 10 µm.

It covers particle size calibration, verification of the size setting, counting efficiency, size resolution, false count rate, maximum particle concentration, sampling flow rate, sampling time, response, the calibration interval and the test report, with informative annexes on the calibration uncertainty, counting efficiency, size resolution, false count rate and response.

Instruments meeting it classify air cleanliness in clean rooms and controlled clean zones, and measure particle number and size distribution in other air. Part 4 of GB/T 29024 and an identical adoption of ISO 21501-4:2007, it was issued on 29 September 2017 and has applied since 1 April 2018.

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Document preview — GB/T 29024.4-2017

National Standard of the People's Republic of China

ICS
19.120
Classification
A 28

Issued by: General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China

Contents

  • Preface
  • Introduction
  • 1 Scope
  • 2 Terms and definitions
  • 3 Requirements
  • 4 test method
  • Appendix A (Informative) Particle size calibration uncertainty assessment
  • Appendix B (informative) counting efficiency
  • Appendix C (informative) Particle size resolution
  • Appendix D (informative) False count rate
  • Appendix E (Informative) Responsiveness
  • References

Foreword

GB/T 29024 "Particle size analysis of single optical measurement method" is divided into four parts.

--- Part 1: Light scattering aerosol spectrometer;

--- Part 2: Liquid particle counter light scattering method;

--- Part 3: Liquid particle counter photolithography;

--- Part 4: Clean room light scattering dust particle counter.

This section GB/T 29024 Part 4.

This section drafted in accordance with GB/T 1.1-2009 given rules.

This section uses the translation method is equivalent to using ISO 21501-4:2007 "Particle size analysis of optical measurement methods Part 4: Jie Net interspersed light scattering particle counter ".

This section made the following editorial changes.

--- In keeping with the provisions of Chapter 3, replace "sampling volume" in the first column with "response capacity".

Introduction

In the electronics industry, the pharmaceutical industry, precision instruments manufacturing and medical clinics, and many other areas need to monitor particle pollution, and dust particle meter The counter is an effective instrument for monitoring particulate contamination in the air. This section provides a calibration procedure and test for light-scattering dust particle counters Card method to minimize errors in instrument measurements and differences in measurement results between different instruments.

1 Scope

GB/T 29024 provisions of this part of the clean room light scattering particle counter dust (abbreviated as LSAPC, hereinafter referred to as the count ) Calibration and verification methods, the instrument used to measure the size of particles suspended in the air and the number of concentrations. Light scattering method in this section For single particle measurement, the typical particle size measurement of this method is in the range of 0.1 µm to 10 µm.

In line with this section of the instrument is mainly used for clean rooms and controlled cleanliness of the classification of air cleanliness, see reference [2], but also For other ambient air particles and particle size distribution measurement.

This section contains the following.

--- Particle size calibration;

--- particle size set value verification;

--- Counting efficiency;

--- Particle size resolution;

--- Fake count rate;

--- maximum particle concentration;

--- Sampling flow;

--- sampling time;

--- Responsiveness;

--- Calibration cycle;

---testing report.

2 Terms and definitions

The following terms and definitions apply to this document.

2.1 Calibration particles

Monodisperse spherical particles with a known average particle size. The average particle size can be traceable to the international standard length, and the standard uncertainty should be Not more than 2.5% (such as polystyrene latex particles PSL).

Note The refractive index of the PSL calibration particles is approximately 1.59 at 589 nm (line D in the sodium spectrum) wavelength.

2.2 Counting efficiency

When measuring the same sample, the ratio of the calibrated counter to the standard instrument measurement.

2.3 Particle counter

Using light scattering or extinction method (light resistance method) for particle counting and particle size measurement of the instrument.

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This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 19 pages — is available in the English PDF.

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