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GB/T 22599-2008Water treatment chemicals - Determination of arsenic content (English PDF)

水处理化学品 砷含量测定方法

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Issued by

General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China; Standardization Administration of China

Level / Type

National · Recommended

Issue date

December 23, 2008

Implementation date

September 1, 2009

Scope

GB/T 22599-2008 is the English-translated version of 水处理化学品 砷含量测定方法.

GB/T 22599-2008 specifies two methods for determining the arsenic content of water treatment chemicals, as a general test method called up by the individual product standards.

The silver diethyldithiocarbamate spectrophotometric method reduces arsenic with zinc to arsine, absorbs it in a pyridine solution of Ag(DDTC) and measures the absorbance at 540 nm against a calibration curve; it applies to test solutions containing 1 µg to 20 µg of arsenic (as As).

The arsenic spot method reduces As(V) to As(III) with potassium iodide and stannous chloride, generates arsine with zinc and compares the brownish-yellow stain on mercuric bromide test paper with a series of standard stains; it applies to 1 µg to 5 µg of arsenic.

For each method the standard sets out the reagents, the glassware cleaning and test apparatus with dimensioned figures, the preparation of test and blank solutions, the procedure and the evaluation of results, leaving the final calculation formula to the product standard.

It was issued on 23 December 2008 and has been in force since 1 September 2009. Classification: ICS 71.040.40, CCS G76. The document runs to 6 pages, delivered complete in English translation.

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Document preview — GB/T 22599-2008

National Standard of the People's Republic of China

ICS
71.040.40
Classification
G76

Issued by: General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China; Standardization Administration of China

Contents

  • Foreword
  • 1 Scope
  • 2 Normative references
  • 3 Silver diethyldithiocarbamate spectrophotometry
  • 4 Arsenic spot method

3 Silver diethyldithiocarbamate spectrophotometry

4 Arsenic spot method

Foreword

This standard was proposed by the China Petroleum and Chemical Industry Association.

This standard is under the jurisdiction of the Water Treatment Agents Sub-committee of the National Technical Committee for Chemical Standardization (SAC/TC 63/SC 5).

Drafting organisation responsible for this standard: CNOOC Tianjin Chemical Research and Design Institute.

Main drafters of this standard: Li Lin, Shao Hongqian, Bai Ying.

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This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 6 pages — is available in the English PDF.

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Editions of GB/T 22599

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GB/T 22599-2008Water treatment chemicals - Determination of arsenic contentcurrent editionCurrent

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