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GB 1886.204-2016Food additive -- Oil of mentha arvensis partially dementholized (English PDF)

食品安全国家标准 食品添加剂 亚洲薄荷素油

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Issued by

National Health and Family Planning Commission

Level / Type

National · Mandatory

Issue date

August 31, 2016

Implementation date

January 1, 2017

Scope

GB 1886.204-2016 is the English-translated version of 食品安全国家标准 食品添加剂 亚洲薄荷素油.

GB 1886.204-2016 — This standard applies to l- limonene as raw materials by a chemical reaction, or caraway oil as raw material obtained from a single food additive incense d-Celery ketone.

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Document preview — GB 1886.204-2016

National Standard of the People's Republic of China

Classification
X 44
Replacing
GB 8319-2003

Issued by: National Health and Family Planning Commission

Contents

  • 1 Scope
  • 2 Chemical name, molecular formula, molecular mass and structural formula
  • 2.1 Chemical Name
  • 2.3 Formula
  • 2.4 Relative molecular mass
  • 3 Technical requirements
  • 3.1 Sensory requirements
  • 3.2 Physical and Chemical Indicators

1 Scope

This standard applies to l- limonene as raw materials by a chemical reaction, or caraway oil as raw material obtained from a single food additive incense d-Celery ketone.

2 Chemical name, molecular formula, molecular mass and structural formula

2.1 Chemical Name

d-1- methyl-4-isopropenyl-6-cyclohexyl-2-one Formula 2.2 C10H14O

2.3 Formula

2.4 Relative molecular mass

150.22 (according to 2007 international relative atomic mass)

3 Technical requirements

3.1 Sensory requirements

Sensory requirements shall comply with the requirements of Table 1.

Table 1 Sensory requirements

Project requires test methods Colorless to pale yellow color Liquid state the sample was placed in a cuvette, were visually observed Aroma caraway (caraway) like aroma GB/T 14454.2 GB 1886.205-2016

3.2 Physical and Chemical Indicators

Physical and chemical indicators should be consistent with the provisions of Table 2.

Table 2. Physical and chemical indicators

Item Index Test Method Solubility (25 °C) 1mL sample soluble in 5mL60% (volume fraction) ethanol GB/T 14455.3 d- carvone content, w /% >= 95.0 Appendix A Refractive index (20 °C) 1.496 ~ 1.502 GB/T 14454.4 the relative density (25 °C/25 °C) 0.955 ~ 0.960 GB/T 11540 Optical rotation (25 °C) 50 ° ~ 60 ° GB/T 14454.5 GB 1886.205-2016 Appendix A Determination of d- carvone content A.1 instruments and equipment A.1.1 chromatograph. According to GB/T 11538-2006 provisions in Chapter 5.

A.1.2 Column. capillary column.

A.1.3 Detector. Hydrogen flame ionization detector.

A.2 Determination

Area normalization method. According to GB/T 11538-2006 10.4 Determination.

A.3 repeatability and results are shown According to GB/T 11538-2006 provisions in 11.4, shall comply with the requirements.

Food Additives d- carvone gas chromatograph and operating conditions, see Appendix B.

GB 1886.205-2016

Appendix B

Food Additives d- carvone gas chromatograph and operating conditions (Area normalization method) B.1 food additives d- carvone gas chromatogram Food Additives d- carvone gas chromatography is shown in Figure B.1.

Figure B.1 food additives d- carvone gas chromatogram

B.2 operating conditions B.2.1 Column. capillary column length 60m, an inner diameter of 0.25mm.

B.2.2 stationary phase. Polyethylene glycol 20000.

B.2.3 film thickness. 0.25µm.

B.2.4 chromatography oven temperature. 150 °C constant temperature.

B.2.5 Inlet temperature. 250 °C.

B.2.6 detector temperature. 300 °C.

B.2.7 Detector. Hydrogen flame ionization detector.

B.2.8 carrier gas. nitrogen.

Before B.2.9 column pressure. 96kPa.

B.2.10 Injection volume. 0.2µL.

B.2.11 Split ratio. 100.1.

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This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 5 pages — is available in the English PDF.

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