DZ/T 0276.13-2015Regulation for testing the physical and mechanical properties of rock. Part 13: Test for determining the specific beat of rock (English PDF)
岩石物理力学性质试验规程 第13部分:岩石比热试验 清晰版
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Issued by
Ministry of Land and Resources
Level / Type
National · Recommended
Issue date
February 4, 2015
Implementation date
April 1, 2015
Scope
DZ/T 0276.13-2015 is the English-translated version of 岩石物理力学性质试验规程 第13部分:岩石比热试验 清晰版.
DZ/T 0276.13-2015 — This part of DZ/T 0276 specifies the differential scanning calorimetry (DSC) method for the determination of rock specific heat. This section applies to the rock specific heat test in rock physics and mechanics tests.
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Document preview — DZ/T 0276.13-2015
National Standard of the People's Republic of China
- ICS
- 19.020
- Classification
- D 00
- Replacing
- DY-94
Issued by: Ministry of Land and Resources
Contents
- Foreword
- 1 Scope
- 2 Normative references
- 3 Terms and definitions
- 4 Principle
- 5 Instruments and reagents
- 5.1 Instrumentation
- 5.2 Reagents
Foreword
DZ/T 0276 "Testing Procedures for Physical and Mechanical Properties of Rocks" is divided into 31 parts.
--- Part 1. General and general provisions;
--- Part 2. Rock moisture test;
--- Part 3. Rock particle density test;
--- Part 4. Rock density test;
---Part 5. Rock water absorption test;
---Part 6. Rock hardness test;
--- Part 7. Rock gloss test;
--- Part 8. Rock antifreeze test;
---Part 9. Rock resistance to disintegration test;
--- Part 10. Rock expansion test;
--- Part 11. Rock erosion test;
--- Part 12. Rock acid and alkali resistance test;
--- Part 13. Rock specific heat test;
--- Part 14. Rock thermal conductivity test;
---Part 15. Rock breakdown voltage and breakdown strength test;
---Part 16. Rock volume resistivity and surface resistivity test;
--- Part 17. Rock radioactivity specific activity test;
---Part 18. Rock uniaxial compressive strength test;
---Part 19. Rock uniaxial compression deformation test;
--- Part 20. Rock triaxial compression strength test;
--- Part 21. Rock tensile strength test;
--- Part 22. Rock flexural strength test;
--- Part 23. Rock point load strength test;
--- Part 24. Rock acoustic wave velocity test;
---Part 25. Rock shear strength test;
--- Part 26. Rock mass deformation test (bearing plate method);
--- Part 27. Rock mass deformation test (drilling deformation method);
---Part 28. Rock mass strength test (direct shear test);
--- Part 29. Rock mass strength test (bearing plate method);
--- Part 30. Rock mass bolt load test;
--- Part 31. Rock sound wave velocity test.
This part is the 13th part of DZ/T 0276.
This part is drafted in accordance with the rules given in GB/T 1.1-2009.
This part replaces DY-94 "Testing procedures for physical and mechanical properties of rocks 9. Specific heat test". This part is compared with DY-94, the main technology the changes are as follows.
--- Added three chapters of "normative reference documents", "terms and definitions", and "principles";
--- Added weighing plate equipment;
--- Added standard samples;
--- Increased the number of samples required;
--- Added an informative appendix on the specific heat value of the reference material under different temperature conditions;
--- Added an informative appendix on the specific heat value of water under different temperature conditions;
--- Modified the balance weighing range;
--- Modified the DSC curve;
--- Modified the specific heat test record table.
This part is proposed by the Ministry of Land and Resources of the People's Republic of China.
This part is under the jurisdiction of the National Land Resources Standardization Technical Committee (SAC/TC93).
This section drafted by. Hubei Institute of Geological Experiments.
1 Scope
This part of DZ/T 0276 specifies the differential scanning calorimetry (DSC) method for the determination of rock specific heat.
This section applies to the rock specific heat test in rock physics and mechanics tests.
2 Normative references
The following documents are indispensable for the application of this document. For dated references, only the dated version applies to this article.
Pieces. For undated references, the latest edition (including all amendments) applies to this document.
DZ/T 0276.2 Test procedures for physical and mechanical properties of rocks - Part 2. Rock moisture test
3 Terms and definitions
The following terms and definitions apply to this document.
Specific heat
The mass of rock sample per unit mass rises or decreases the heat required by 1 ° C, which indicates the ability of the rock to store heat.
4 Principle
The rock sample is compared with the heat signal of the standard sample (known specific heat value) under temperature program control to determine the ratio of the sample.
Calorific value.
5 Instruments and reagents
5.1 Instrumentation
5.1.1 Thermal synthesis analyzer.
5.1.2 Balance. The maximum weighing value is.200g, and the reading accuracy is 0.0001g.
5.1.3 Drying oven. The temperature can be controlled within the range of 75 °C ± 5 °C.
5.1.4 Dryer.
5.1.5 Bending device.
5.1.6 Two sizes and equal quality aluminum discs. one is sealed as a reference disc and the other is capped but not sealed as a sample pan.
5.2 Reagents
Standard sample. alpha-Al 2 O 3 having a purity of 99.9% or more.
......
This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 7 pages — is available in the English PDF.
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Related Standards
DZ/T 0276.1-2015 — Regulation for testing the physical and mechanical properties of rock. Part 1: General rules and regulations
DZ/T 0276.10-2015 — Regulation for testing the physical and mechanical properties of rock. Part 10: Test for determining the swelling property of rock
DZ/T 0276.11-2015 — Regulation for testing the physical and mechanical properties of rock. Part 11: Test for determining the dissolution of rock
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